TC

TC3005: Instrumental Methods of Chemical Analysis syllabus for TC 2021 regulation (Professional Elective-I)

Instrumental Methods of Chemical Analysis detailed syllabus for Textile Chemistry (TC) for 2021 regulation curriculum has been taken from the Anna Universities official website and presented for the TC students. For course code, course name, number of credits for a course and other scheme related information, do visit full semester subjects post given below.

For Textile Chemistry 5th Sem scheme and its subjects, do visit TC 5th Sem 2021 regulation scheme. For Professional Elective-I scheme and its subjects refer to TC Professional Elective-I syllabus scheme. The detailed syllabus of instrumental methods of chemical analysis is as follows.

Course Objectives:

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Unit I

UV – VIS, INFRA RED SPECTROSCOPY 9
UV – VIS spectroscopy – Theory, Franck – Condon principle, Electronic transitions, Deviations from Beer’s law – Instrumentation (block diagram only) – Applications. Infra red spectroscopy – Theory, Fundamental vibrations, Hook’s law – Instrumentation (block diagram only)- Finger print region -Vibrations involved in H2O and CO2 – Applications.

Unit II

NMR, MASS SPECTROSCOPY 9
NMR spectroscopy – Theory, Relaxation Process – Instrumentation (block diagram only) -Chemical shift – Internal standard – TMS – Shielding and De- Shielding Effects – Factors influencing Chemical shift – Applications. Mass spectroscopy: Theory, Instrumentation (block diagram only) – Ionization Techniques – Electron impact ionization, Chemical ionization and Desorption techniques. Nirogen rule, McLafferty rearrangement.

Unit III

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Unit IV

CHROMATOGRAPHIC TECHNIQUES 9
Chromatographic Techniques – Introduction – classification – Theory, Instrumentation and Applications of Paper Chromatography, Thin Layer Chromatography, Column Chromatography, High Performance Liquid Chromatography and Gas – Liquid Chromatography.

Unit V

PRECISION AND ACCURACY 9
Errors, Precision and Accuracy: Definitions, Significant figures – Types of Errors – Methods of expressing accuracy and precision , Confidence limits.

Course Outcomes:

Upon completion of the course, the students

  1. Theory and Instruments of UV – VIS, Infra red spectroscopy.
  2. Theory and Instruments of NMR, Mass spectroscopy.
  3. Potentiometric measurements, Thermogravimeter, Differential Thermal Analysis.
  4. Chromatographic Techniques.
  5. Precision, accuracy and errors in analytical instruments

Text Books:

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Reference Books:

  1. Bona,M., “Modern control Techniques in textile finishing and making up”, Eurotex, Blachwells Bookshop, London, 2001
  2. Banwell,G.C., “Fundamentals of molecular spectroscopy”, TMH, 2003.

For detailed syllabus of all the other subjects of Textile Chemistry 5th Sem, visit TC 5th Sem subject syllabuses for 2021 regulation.

For all Textile Chemistry results, visit Anna University TC all semester results direct link.

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