Pharmaceutical Analysis Laboratory detailed syllabus for Pharmaceutical Technology (Pharma Tech) for 2019 regulation curriculum has been taken from the Anna Universities official website and presented for the Pharma Tech students. For course code, course name, number of credits for a course and other scheme related information, do visit full semester subjects post given below.
For Pharmaceutical Technology 4th Sem scheme and its subjects, do visit Pharma Tech 4th Sem 2019 regulation scheme. The detailed syllabus of pharmaceutical analysis laboratory is as follows.
Course Objective:
The course aims to,
- carry out analytical experiments related to spectroscopic and chromatographic techniques.
- enable students to learn the principles of analysis for pharmaceutical applications
List of Experiments:
- Standardization of analytical weights and calibration of volumetric apparatus.
- Experiments involving titrimetric methods (permanganometry, iodometry, iodimetry, complexometry, non aqueous).
- Experiments involving gravimetric analysis.
- Determination of impurities by limit test: chloride, sulphate, iron, arsenic.
- Determination of Amax.
- Validation of beer Lamberts law.
- Quantitative and qualitative analysis of drug molecule using standard comparison method by UV/Vis spectroscopy.
- Quantitative analysis by fluorimetry.
- Analysis of drug molecule using standard comparison method by HPLC.
- Interpretation of IR, NMR spectra.
- Separation of components using paper, TLC and column chromatography.
List of Equipment
FOR BATCH OF 30 STUDENTS
- Hot air oven
- pH meter
- UV-Visible spectrophotometer
- HPLC
- Fluorimetry
- Arsenic limit test apparatus
- Water bath
- Weighing balance
Course Outcome:
At the end of the course the students will be able to
- study and analyse the monograph of different drugs.
- characterize and analyze different sources of impurities.
- quantify and interpret drug moieties using advanced methods.
References:
- Atherden L.M, “Bentley and Driver”s Textbook of Pharmaceutical Chemistry”, 8th Edition, Oxford University Press, 2004.
- Siddiqui, Anees A, “Pharmaceutical Analysis”. Vol.I& II, 3rd edition, CBS Publishers, 2014.
- Takeru Higuchi, Einar Brochmann, Hanffen Hanssen, Hamffen Hanssen, “Pharmaceutical Analysis” 1st Edition, CBS Publishers, 2005.
- Loyd V. Allen Jr, “Remington: The Science and Practice of Pharmacy”. Vol. I and II, 22nd Edition, Pharmaceutical Press;, 2012.
- Kenneth A. Connors, “Textbook of Pharmaceutical Analysis”, 3rd Edition, John wiley and sons, New York, 2007.
For detailed syllabus of all other subjects of Pharmaceutical Technology, 2019 regulation curriculum do visit Pharma Tech 4th Sem subject syllabuses for 2019 regulation.
For all Pharmaceutical Technology results, visit Anna University Pharma Tech all semester results direct link.