Instrumental Methods of Analysis detail syllabus for Chemical & Electrochemical Engineering (Che Eleche), 2017 regulation is taken from Anna University official website and presented for students of Anna University. The details of the course are: course code (CH8491), Category (PC), Contact Periods/week (3), Teaching hours/week (3), Practical Hours/week (0). The total course credits are given in combined syllabus.
For all other che eleche 5th sem syllabus for b.tech 2017 regulation anna univ you can visit Che Eleche 5th Sem syllabus for B.Tech 2017 regulation Anna Univ Subjects. The detail syllabus for instrumental methods of analysis is as follows.”
Course Objective:
- To know the principle and importance of various analytical instruments used for the characterization of various materials
Unit I
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Unit II
Qualitative Analysis By Uv and Visible Spectrocopy
Lamda max and epsilon max rules, Woodward -Fieser rules for the calculation of absorption maxima (Lamda max) for dienes and carbonyl compounds, Effects of auxochromes and effects of conjugation on the absorption maxima, Different shifts of absorption peaks(Bathochromic, hypsochromic, hypochromic), Instrumentation for UV and Visible spectrophotometers (source, optical parts and detectors), Applications of UV and Visible spectroscopy.
Unit III
Quantitativeanalysis By Uv and Visible Spectrocopy
Beer-Lamberts law, limitations, deviations (real, chemical, instrumental), estimation of inorganic ions such as Fe, Ni and estimation of nitrite using Beer -Lamberts law, multicomponent analysis (no overlap, single way overlap and two way overlap), photometric titration(experimental set -up and various types of titrations and their corresponding curves).
Unit IV
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Unit V
Chromatographic Methods
Classification of chromatographic methods, column, thin layer, paper, gas, High Performance Liquid Chromatographical methods (principle, mode of separation and technique).
Course Outcome:
- To have thorough understanding of theory, instrumentation and applications of analytical equipments used in industries for testing quality of raw materials, intermediates and finished products. To know the importance of analytical instrumentation during the purification, compounding and formulating the finished product.
Text Books:
- Sivasankar B., Instrumental Methods of Analysis, Oxford University Press, 2012.
- William Kemp, Organic Spectroscopy, 3rd Edition, Palgrave publishers, 2007.
References:
- Douglas A. Skoog, F. James Holler, Stanley R. Crouch, Instrumental Analysis, CENGAGE Learning, India, 7th Edition, 2007.
- Willard H.H, Merritt L.L, Dean J.A and Settle F.A, Instrumental method of analysis, 7th edition, Wadsworth Publishing Company, 1988.
- Gurdeep R. Chatwal, Sharma K. Anand, Instrumental methods of Chemical Analysis, Himalaya Publishers, New Delhi, 2014
- John R Dyer, Applications of Absorption Spectroscopy of Organic Compounds, Prenticehall of India Pvt. Ltd., 2012
- Robert M. Silverstein, Francis X. Webstrer, David Kiemle, David L. Bryce, Spectrometric Identification of Organic Compounds, Wiley, 8th Edition, 2010.
For detail syllabus of all other subjects of B.Tech Che Eleche, 2017 regulation do visit Che Eleche 5th Sem syllabus for 2017 Regulation.
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