EL3412: Electrochemistry Laboratory syllabus for CEE 2021 regulation

Electrochemistry Laboratory detailed syllabus for Chemical & Electrochemical Engineering (CEE) for 2021 regulation curriculum has been taken from the Anna University official website and presented for the CEE students. For course code, course name, number of credits for a course and other scheme related information, do visit full semester subjects post given below.

For Chemical & Electrochemical Engineering 4th Sem scheme and its subjects, do visit CEE 4th Sem 2021 regulation scheme. The detailed syllabus of electrochemistry laboratory is as follows.

Course Objectives:

• To enable the students to develop a sound working knowledge on different types of electrochemical techniques and electrochemical parameter calculations.

List of Experiments:

1. Fabrication of Reference electrode (Ag/AgCl) and its validation
2. Fabrication of modified electrodes and calculation of surface excess
3. Potentiometric titration of redox couple (Fe/Ce ions)
4. Estimation of equilibrium potential of quinhydrone electrode(pH dependence)
5. Determination of formal potential and diffusion coefficient for a reversible process using ferricyanide and ferrocyanide
6. Distinguish between inner and outer sphere processes using Pt and glassy carbon electrode
7. Effect of dissolved oxygen in electrochemical reduction of nitrophenol
8. Amperometric method for sensing hydrogen peroxide
9. Determination of dihydroxy phenols using cyclic voltammetry
10. Investigation of electrochromism using electropolymerisation on a ITO substrate
11. Double-layer capacitance measurement using cyclic voltammetry
12. Electrode surface area measurement using a redox probe.

Course Outcomes:

Upon completion of the course, the students would be able to

• Calculate electrochemical parameters from various electrochemical techniques.
• Apply the standard procedures to carry out an electrochemical experiment.

List of Equipments:

FOR BATCH OF 30 STUDENTS

1. Electrochemical analyzer- 1 No.
2. Potentiometer- 3 No.
3. Glassy carbon electrode- 15 No.
4. ITO electrode-15 No.
5. Reference electrode- 15No.
6. Pt electrode- 15 No.

For detailed syllabus of all other subjects of Chemical & Electrochemical Engineering, 2021 regulation curriculum do visit CEE 4th Sem subject syllabuses for 2021 regulation.

For all Chemical & Electrochemical Engineering results, visit Anna University CEE all semester results direct link.