Instrumental Methods of Analysis detailed syllabus for Chemical & Electrochemical Engineering (CEE) for 2021 regulation curriculum has been taken from the Anna University official website and presented for the CEE students. For course code, course name, number of credits for a course and other scheme related information, do visit full semester subjects post given below.
For Chemical & Electrochemical Engineering 3rd Sem scheme and its subjects, do visit CEE 3rd Sem 2021 regulation scheme. The detailed syllabus of instrumental methods of analysis is as follows.
Course Objectives:
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Unit I
INTRODUCTION TO SPECTROSCOPICAL METHODS OF ANALYSIS 9 Electromagnetic radiation: various ranges, dual properties, various energy levels, interaction of photons with matter, absorbance & transmittance and their relationship, permitted energy levels for the electrons of an atom and simple molecules, various electronic transitions in organic and inorganic compounds effected by UV, and visible radiations, various energy level diagrams of saturated, unsaturated and carbonyl compounds, excitation by UV and visible radiations, choice of solvents, cut off wavelengths for solvents
Unit II
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Unit III
QUANTITATIVEANALYSIS BY UV AND VISIBLE SPECTROCOPY 9 Beer-Lambert’s law, limitations, deviations (real, chemical, instrumental), estimation of inorganic ions such as Fe, Ni and estimation of nitrite using Beer -Lambert’s law, multicomponent analysis (no overlap, single way overlap and two way overlap), photometric titration(experimental set -up and various types of titrations and their corresponding curves).
Unit IV
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Unit V
CHROMATOGRAPHIC METHODS 9 Classification of chromatographic methods, column, thin layer, paper, gas, High Performance Liquid Chromatographical methods (principle, mode of separation and technique).
Course Outcomes:
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Text Books:
- Sivasankar B., Instrumental Methods of Analysis, Oxford University Press, 2012.
- William Kemp, Organic Spectroscopy, 3rd Edition, Palgrave publishers, 2007.
Reference Books:
- Douglas A. Skoog, F. James Holler, Stanley R. Crouch, Instrumental Analysis, CENGAGE Learning, India, 7th Edition, 2007.
- Willard H.H, Merritt L.L, Dean J.A and Settle F.A, Instrumental method of analysis, 7th edition, Wadsworth Publishing Company, 1988.
- Gurdeep R. Chatwal, Sharma K. Anand, Instrumental methods of Chemical Analysis, Himalaya Publishers, New Delhi, 2014
- John R Dyer, Applications of Absorption Spectroscopy of Organic Compounds, Prentice-hall of India Pvt. Ltd., 2012
- Robert M. Silverstein, Francis X. Webstrer, David Kiemle, David L. Bryce, Spectrometric Identification of Organic Compounds, Wiley, 8th Edition, 2010.
For detailed syllabus of all other subjects of Chemical & Electrochemical Engineering, 2021 regulation curriculum do visit CEE 3rd Sem subject syllabuses for 2021 regulation.
For all Chemical & Electrochemical Engineering results, visit Anna University CEE all semester results direct link.