Analytical Instrumentation detailed syllabus for Instrumentation & Control Engineering (ICE) for 2021 regulation curriculum has been taken from the Anna Universities official website and presented for the ICE students. For course code, course name, number of credits for a course and other scheme related information, do visit full semester subjects post given below.
For Instrumentation & Control Engineering 5th Sem scheme and its subjects, do visit ICE 5th Sem 2021 regulation scheme. For Professional Elective-IV scheme and its subjects refer to ICE Professional Elective-IV syllabus scheme. The detailed syllabus of analytical instrumentation is as follows.
Course Objectives:
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Unit I
SPECTROPHOTOMETRY
Spectral methods of analysis – Beer-Lambert law – UV-Visible spectroscopy – IR Spectrophotometry – FTIR spectrophotometry – Atomic absorption spectrophotometry – Flame emission and atomic emission photometry – Construction, working principle, sources detectors and applications.
Unit II
CHROMATOGRAPHY
General principles – classification – chromatographic behaviour of solutes – quantitative determination – Gas chromatography – Liquid chromatography – High-pressure liquid chromatography – Applications.
Unit III
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Unit IV
pH METERS AND DISSOLVED COMPONENT ANALYZERS
Selective ion electrodes – Principle of pH and conductivity measurement – dissolved oxygen analyzer – Sodium analyzer – Silicon analyzer – Water quality Analyzers.
Unit V
NUCLEAR MAGNETIC RESONANCE AND MASS SPECTROMETRY
NMR – Basic principles – Continuous and Pulsed Fourier Transform NMR spectrometer – Mass Spectrometry – Sample system – Ionization methods – Mass analyzers – Types of mass spectrometry.
Skill Development Activities
(Group Seminar/Mini 10
Project/Assignment/Content Preparation / Quiz/ Surprise Test / Solving GATE questions/ etc)
- A seminar on applications of various analytical techniques.
- Selection of Chromatography for applications.
- Familiarization of any one relevant software tool (MATLAB/ SCILAB/ LABVIEW/ Proteus/ Equivalent open source software)
- Realization of spectroscopy and analyzers in hardware
- Introduction to other advanced spectroscopy and analyzer not covered in the above syllabus
Course Outcomes:
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Text Books:
- Braun, R.D., �Introduction to Instrumental Analysis�, Pharma Book Syndicate, Singapore, 2nd edition 2016.
- Willard, H.H., Merritt, L.L., Dean, J.A., Settle, F.A.,�Instrumental methods of analysis�, CBS publishing & distribution, 7th Edition, 2012.
- Robert E. Sherman., �Analytical Instrumentation, Instruments�, Society of America, 1996.
Reference Books:
- Khandpur, R.S., �Handbook of Analytical Instruments�, Tata McGraw Hill publishing Co. Ltd., 5th edition 2018.
- Ewing, G.W., �Instrumental Methods of Chemical Analysis�, McGraw Hill, 5th edition reprint 1985. Digitized in May 2013.
- Liptak, B.G., �Process Measurement and Analysis�, CRC Press, 5th Edition, 2016.
- NPTEL lecture notes on, �Modern Instrumental methods of Analysis� by Dr.J.R. Mudakavi, IISC, Bangalore
List of Open Source Software/ Learning Website:
- https://nptel.ac.in/courses/103108100
- https://nptel.ac.in/courses/103108139
- https://instrumentationtools.com/oxygen-analyzer-working-principle/
- https://www.excedr.com/blog/spectrometer-vs-spectrophotometer/
- https://nptel.ac.in/courses/104106122
- http://www.premierbiosoft.com/tech_notes/mass-spectrometry.html
- https://chem.libretexts.org/Bookshelves/Analytical_Chemistry/Supplemental_Modules_(Analytica l_Chemistry)/Instrumental_Analysis/Chromatography/Gas_Chromatography
- https://www.waters.com/nextgen/in/en/education/primers/beginner-s-guide-to-liquid-chromatography.html
For detailed syllabus of all the other subjects of Instrumentation & Control Engineering 5th Sem, visit ICE 5th Sem subject syllabuses for 2021 regulation.
For all Instrumentation & Control Engineering results, visit Anna University ICE all semester results direct link.