Chemical Analysis Laboratory detail syllabus for Petroleum Engineering (Petro Engg), 2017 regulation is taken from Anna University official website and presented for students of Anna University. The details of the course are: course code (CH8281), Category (BS), Contact Periods/week (4), Teaching hours/week (0), Practical Hours/week (0). The total course credits are 4.
For all other petro engg 4th sem syllabus for b.tech 2017 regulation anna univ you can visit Petro Engg 4th Sem syllabus for B.Tech 2017 regulation Anna Univ Subjects. The detail syllabus for chemical analysis laboratory is as follows.”(Minimum of 8 experiments to be conducted)
Course Objective:
- To make the student acquire practical skills in the wet chemical and \ instrumentalmethods for quantitative estimation of nitrite in water, cement, oil, coal and Phenol.
List of Experiments:
- Determination of Redwood / Saybolt numbers, kinematic viscosity and viscosity index of Lubricating oils
- Determination of flash point, fire point, cloud and pour point of oils
- Determination of acid value and iodine value of oils
- Determination of COD of water samples
- Cement Analysis a. Estimation of silica content b. Estimation of mixed oxide content c. Estimation of calcium oxide content d. Estimation of calcium oxide by rapid method
- Coal Analysis a. Estimation of sulphur present in coal b. Ultimate analysis of coal c. Proximate analysis of coal
- Soap Analysis a. Estimation of total fatty acid b. Estimation of percentage alkali content
- Flue gas analysis by Orsats apparatus
- Estimation of phenol.
- Determination of calorific value using bomb calorimeter
- Determination of nitrite in water.
List of Equipment:
S. No. Description of Equipment Qty.
- Silica Crucible 20
- Heating Mantle 3
- Muffle Furnace 1
- Hot air oven 1
- Desiccator 5
- Vacuum Pump 1
- Condenser 10
- Reflux Condenser 10
- Pensky martens closed cup apparatus 1
- Cleveland Open cup apparatus 1
- Cloud point apparatus 1
- Saybolt Viscometer 1
- Redwood Viscometer 1
- Bomb Calorimeter 1
- COD reflux 1
- Orsat apparatus 1
- UV-Vis Spectrophotometer 1
Course Outcome:
- Familiarization with equipment like viscometers, flash and fire point apparatus etc
- Familiarization of methods for determining COD
- Familiarization of a few simple synthetic techniques for soap
References:
- Environmental pollution analysis, S.M.Khopkar, New age international. 2011
- Manual of environmental analysis, N.C Aery, Ane books. 2010
- Text book of quantitative chemical analysis, J.Mendham, Pearson education 2008
For detail syllabus of all other subjects of B.Tech Petro Engg, 2017 regulation do visit Petro Engg 4th Sem syllabus for 2017 Regulation.
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