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Anna University B.Tech PL (R13) 5th Sem Polymer Preparation and Characterization Laboratory Detailed Syllabus

Polymer Preparation and Characterization Laboratory Syllabus for B.Tech 5th sem is covered here. This gives the details about credits, number of hours and other details along with reference books for the course.

The detailed syllabus for Polymer Preparation and Characterization Laboratory B.Tech (R13) fifthsem is as follows

OBJECTIVES: To prepare the students with Methodology for facing the Industrial and academic challenges in

  • Identifying various polymers
  • Controlling the quality of incoming raw materials and processing
  • Analyzing polymers through various instrumental methods

LIST OF EXPERIMENTS

  • Part A Preparation
  • Preparation of phenol – formaldehyde (Novalac) resin.
  • Preparation of phenol – formaldehyde (Resol) resin.
  • Preparation of Urea formaldehyde resin.
  • Preparation of Bisphenol – An epoxy resin.
  • Bulk polymerization of styrene.
  • Regneration of Cellulose
  • Emulsion Polymerization of styrene.
  • Solution Polymerization of acrylonitrile.
  • Suspension Polymerization of Methyl methacrylate.
  • Interfacial Polymerization of heamethylene diamine and sebacoyl chloride
  • Copolymerization of styrene and methyl methacrylate.
  • Ring opening polymerization of Caprolactone
    (Any seven of the above)

Part B Characterization

  • Determination of molecular weight by end group analysis (COOH group)
  • Determination of molecular weight of polymers by viscosity method.

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TOTAL : 45 PERIODS

OUTCOMES: Upon completing this course, the students

  • Will acquire skills in preparation of polymers using various polymerization techniques.
  • Will develop the conversion of polymeric materials into product.
  • Will be able to characterize the resin behavior.

LIST OF EQUIPMENT FOR BATCH OF 30 STUDENTS

  • Magnetic stirrer 10 Nos.
  • Thermostatic Water bath 2 Nos.
  • Vacuum Pump 1 No
  • Heating Mantle 8 Nos.
  • Water distillation set up 1 No
  • Bunsen burner 15 Nos.
  • Electronic balance 2 Nos.
  • Air oven 1 No
  • Melting point apparatus 1 No
  • Retard stands 15 Nos.
  • Burette
  • Pipette
  • Funnel

For all other B.Tech PL 5th sem syllabus go to Anna University B.Tech POLYMER TECHNOLOGY (PL) 5th Sem Course Structure for (R13) Batch.All details and yearly new syllabus will be updated here time to time. Subscribe, like us on facebook and follow us on google plus for all updates.

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