Analytical Instruments detail syllabus for Electronics & Instrumentation Engineering (Eie), 2017 regulation is taken from Anna University official website and presented for students of Anna University. The details of the course are: course code (EI8551), Category (PC), Contact Periods/week (3), Teaching hours/week (3), Practical Hours/week (0). The total course credits are given in combined syllabus.
For all other eie 5th sem syllabus for be 2017 regulation anna univ you can visit Eie 5th Sem syllabus for BE 2017 regulation Anna Univ Subjects. The detail syllabus for analytical instruments is as follows.”
Course Objective:
- To understand the theory and operational principles of instrumental methods for identification and quantitative analysis of chemical substances by different types of spectroscopy.
- To impart fundamental knowledge on gas chromatography and liquid chromatography.
- To integrate a fundamental understanding of the underlining principles of physics as they relate to specific instrumentation used for gas analyzers and pollution monitoring instruments.
- To understand the working principle, types and applications of NMR and Mass spectroscopy.
To impart knowledge on the important measurement in many chemical processes and laboratories handling liquids or solutions.
Unit I
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Unit II
Chromatography
General principles – classification – chromatographic behavior of solutes – quantitative determination – Gas chromatography – Liquid chromatography – High-pressure liquid chromatography -Applications.
Unit III
Industrial Gas Analyzers and Pollution Monitoring Instruments
Gas analyzers – Oxygen, NO2 and H2S types, IR analyzers, thermal conductivity detectors, analysis basedonionizationofgases.
Air pollution due to carbon monoxide, hydrocarbons, nitrogen oxides, sulphur dioxide estimation – Dust andsmoke measurements.
Unit IV
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Unit V
Nuclear Magnetic Resonance and Mass Spectrometry
NMR – Basic principles – Continuous and Pulsed Fourier Transform NMR spectrometer -Mass Spectrometry – Sample system -Ionization methods -Mass analyzers -Types ofmass spectrometry.
Course Outcome:
- Ability to understand the fundamental principles of selective analytical instruments used in medical diagnosis, quality assurance& control and research studies.
- Abilityto assess and suggest a suitable analytical method for a specific purpose, and evaluate sensitivity, important sources of interferences and errors, and also suggest alternative analytical methods for quality assurance.
- Ability to critically evaluate the strengths and limitations of the various instrumental methods.
- Ability to develop critical thinking for interpreting analytical data.
- Ability to understandthe working principle, types and applications of NMR and Mass spectroscopy
Text Books:
- Willard, H.H., Merritt, L.L., Dean, J.A., Settle, F.A., Instrumentalmethodsofanalysis, CBS publishing and distribution, 7th Edition, 2012.
- Braun, R.D., Introduction toInstrumentalAnalysis, Pharma Book Syndicate,Singapore, 2006.
- RobertE. Sherman., AnalyticalInstrumentation,InstrumentsSocietyofAmerica, 1996.
References:
- Khandpur, R.S., Handbook of Analytical Instruments, Tata McGraw-Hill publishing Co. Ltd.,2nd Edition 2007.
- Ewing, G.W., Instrumental Methods of Chemical Analysis, McGraw-Hill, 5th Edition reprint 1985. (Digitized in 2007).
- Liptak, B.G., Process Measurement and Analysis, CRC Press, 5th Edition, 2015.
- NPTEL lecture notes on, Modern Instrumental methods of Analysis by Dr.J.R. Mudakavi,IISC, Bangalore.
For detail syllabus of all other subjects of BE Eie, 2017 regulation do visit Eie 5th Sem syllabus for 2017 Regulation.
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