Spectral Analysis Detailed Syllabus for Pharmaceutical Chemistry M.Pharm first year second sem is covered here. This gives the details about credits, number of hours and other details along with reference books for the course.
The detailed syllabus for Spectral Analysis M.Pharm 2017-2018 (R17) first year second sem is as follows.
M.Pharm. I Year II Sem.
Course Objective: The students will acquire the knowledge about the various aspects of X-Ray diffraction methods, all types of IR methods, particle sizing methods, also DSC, DTA, TGA etc
Course Outcome: By the completion of topics the students will come out with the thorough knowledge of various spectral aspects of X-Ray, IR, SEM, ORD etc which help them in further projects works and also industrial opportunities.
UNIT – I : X-Ray diffraction methods: Origin of X-rays, basic aspects of crystals, X-ray crystallography, miller indices, rotating crystal techniques, single crystal diffraction, power diffraction, structural elucidation, and applications.
UNIT – II
- FT-NIR: Principle (overtones, combinations, fermi resonance, interferences etc.), instrumentation (dispersion spectrometer and FT-NIR), advantage, and disadvantage, qualitative and quantitative applications, including PAT and non-destructive analysis.
- ATR: Principle (total internal reflection, evanescent wave, etc.), instrumentation (ATR crystal, IR beam), advantages, and disadvantages, pharmaceutical applications.
UNIT – III : Electrometric Techniques: Principle, instrumentation and applications of Potentiometer, Amperometer, Conductometer and Polarography.
UNIT – IV
- Spectroflourimetry: Theory of Fluorescence, Factors affecting fluorescence (Characteristics of drugs that can be analyzed by flourimetry), Quenchers, Instrumentation, and Applications of fluorescence spectrophotometer.
- Flame emission spectroscopy and Atomic absorption spectroscopy: Principle, Instrumentation, Interferences, and applications.
UNIT – V : FT- Raman: Principle (absorption, diffraction, scattering and emission of wave, molecular interaction), instrumentation (Dispersive Raman, FT-Raman), advantage and disadvantage, pharmaceutical applications including detection of counterfeit
REFERENCES:
- Instrumental Methods of Chemical Analysis by B.K Sharma
- Organic spectroscopy by Y.R Sharma
- A Text book of Pharmaceutical Analysis by Kerrenth A. Connors
- Vogel’s Text book of Quantitative Chemical Analysis by A.I. Vogel
- Practical Pharmaceutical Chemistry by A.H. Beckett and J.B. Stenlake
- Organic Chemistry by I. L. Finar
- Organic spectroscopy by William Kemp
- Quantitative Analysis of Drugs by D. C. Garrett
- Quantitative Analysis of Drugs in Pharmaceutical Formulations by P. D. Sethi
- Spectrophotometric identification of Organic Compounds by Silverstein
- HPTLC by P.D. Seth
- Spectroscopy by Donald L Pavia, Gary M Lampman, George S Kriz, James A Vyvyan
For all other M.Pharm 1st Year 2nd Sem syllabus go to JNTUH M.Pharm Pharmaceutical Chemistry 1st Year 2nd Sem Course Structure for (R17) Batch.
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