Introduction To Analytical Instruments for Chemical Analysis detailed Syllabus for Chemical Engineering (CH), K scheme PDF has been taken from the MSBTE official website and presented for the diploma students. For Subject Code, Subject Name, Lectures, Tutorial, Practical/Drawing, Credits, Theory (Max & Min) Marks, Practical (Max & Min) Marks, Total Marks, and other information, do visit full semester subjects post given below.
For all other MSBTE Chemical Engineering 3rd Sem K Scheme Syllabus PDF, do visit MSBTE Chemical Engineering 3rd Sem K Scheme Syllabus PDF Subjects. The detailed Syllabus for introduction to analytical instruments for chemical analysis is as follows.
Rationale
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Course Outcomes:
Students will be able to achieve & demonstrate the following COs on completion of course based learning
- Differentiate between different instrumental methods of chemical analysis as per requirement.
- Select relevant Spectroscopy based method of analysis based on nature of sample.
- Select appropriate chromatography based analytical instruments for the given analyte.
- Interpret the results of thermoanalytical method to decide the thermal stability of a material
- Identify analytical instruments for composition and crystallographic study of a relevant sample.
Unit I
Introduction to Instrumental Methods of analysis 1.1 Purpose/ Necessity of Chemical analysis and methods of analysis a. Quantitative Analysis b. Qualitative Analysis c. Chemical Methods d. Physical methods 1.2 Differentiate between physical properties and analytical methods of measurement. 1.3 Advantages and limitation of Chemical and Instrumental methods. 1.4 Classification of basic Instrumental method of chemical analysis : a. Electrochemical method b. Optical methods c. Radiometric method d. Mass Spectrometry e. Nuclear Magnetic Resonance. Lecture Using Chalk-Board Presentations Case Study
Unit II
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Unit III
Chromatography 3.1 Introduction of chromatography : Purpose and Principle. 3.2 Difference between spectroscopy and chromatographic based methods. 3.3 Introduction, Principle and Applications of following type of chromatography: a. Adsorption Chromatography b. Partition Chromatography c. Liquid – Liquid Chromatography d. Gas Chromatography(GC) e. Paper Chromatography f. Thin Layer Chromatography (TLC) g. High Performance Liquid Chromatography (HPLC) 3.4 Construction and Working of Gas Chromatography and High Performance Liquid Chromatography. 3.5 Introduction and Application of Gas Chromatography – Mass Spectrometry (GC-MS) and Liquid Chromatography – Mass Spectrometry (LC-MS) Lecture Using Chalk-Board Video Demonstrations Site/Industry Visit Case Study
Unit IV
Thermoanalytical Methods 4.1 Introduction, Principle and Applications of Thermogravimetric method of analysis (TGA). 4.2 Thermoanalytical methods based on thermal characteristics of material : a. Differential Scanning Calorimetry (DSC) b. Differential Thermal analysis (DTA). Lecture Using Chalk-Board Video Demonstrations Case Study
Unit V
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Suggested Learning Materials / Books
- B. K. Sharma Instrumental Method of Chemical Analysis GOEL Publishing House, Meerut (India) ISBN -81-87224-98-3
- Douglas A. Skoog F. James Holler Stanley R. Crouch Principle of Instrumental Analysis Cengage ISBN 9789353506193
- P. C. Jain, Monika Jain Engineering Chemistry Dhanpat Rai Publishing Company,17th Edition ISBN 978-9352160006
- Gurdeep R. Chatwal and Sham K. Anand Instrumental Methods of Chemical Analysis (5th Edition) Himalaya Publishing House ISBN 9789351420880
- R.Gopalan R., K. Rangarajan K., P.S.Subramanian Elements of Analytical Chemistry (3rd Edition) S. Chand & Sons ISBN: 978-81-8054765-2
Learning Websites & Portals
- https://nptel.ac.in/courses/103108100 https://www.youtube.com/watch?v=UHYfgwjE2i4 Introduction to the Modern Instrumental Methods of Analysis by Dr. J.R. Mudakavi
- https://www.youtube.com/watch?v=R_tgHUUXiE4 Common Analytical Instruments
- https://www.youtube.com/watch?v=O39avevqndU Ultraviolet / Visible Spectroscopy (UV-Vis)
- https://www.youtube.com/watch?v=P9iAV-x5y-w The Science Behind UV Vis Spectroscopy: Everything You Need To Know
- https://www.youtube.com/watch?v=uSG8ANBTaN0 Gas Chromatography- Explainer Video
- https://www.youtube.com/watch?v=Wap9pQEN4gE Atomic Absorption Spectroscopy (AAS) Explained
- https://www.youtube.com/watch?v=UycPljfrnWo Quickly Understand Gas Chromatography
- https://www.petro-online.com/news/analytical-instrumentation /11/gr-scientific/water-content-determination-of-crude-oils-and-petroleum-products-by-coulometric-karl-fischer-titration /34652 Water Content Determination of Crude Oils and Petroleum Products by Coulometric Karl Fischer Titration
- https://www.youtube.com/watch?v=QHMzFUo0NL8 What is X-ray Diffraction?
- https://www.iitk.ac.in/che/PG_research_lab/pdf/resources/TGA -DSC-reading-material.pdf Thermal Analysis Thermogravimetry (TG) & Differential Scanning Calorimetry (DSC)
- https://webbook.nist.gov/chemistry NIST chemistry workbook
For detail Syllabus of all other subjects of Chemical Engineering, K scheme do visit Chemical Engineering 3rd Sem Syllabus for K scheme.
For all Chemical Engineering results, visit MSBTE Chemical Engineering all semester results direct links.