Instrumental Methods of Chemical Analysis Petro 3rd Sem Syllabus for VTU BE 2017 Scheme

Instrumental Methods of Chemical Analysis detail syllabus for Petroleum Engineering (Petro), 2017 scheme is taken from VTU official website and presented for VTU students. The course code (17PC34), and for exam duration, Teaching Hr/week, Practical Hr/week, Total Marks, internal marks, theory marks, duration and credits do visit complete sem subjects post given below.

For all other petro 3rd sem syllabus for be 2017 scheme vtu you can visit Petro 3rd Sem syllabus for BE 2017 Scheme VTU Subjects. The detail syllabus for instrumental methods of chemical analysis is as follows.

Course Objectives:

This course enables students to: The various modern analytical techniques like IR spectroscopy, AAS, Flame photometry, Radiochemical, Electrophoretic, Polarography, different chromatographic methods and other important topics are taught to enable the students to understand and apply the principles involved in the determination of different bulk drugs and their formulation. In addition to the theoretical aspects, the basic practical knowledge relevant to the analysis is also imparted.

Module 1
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Module 2

Radiochemical Techniques – Define radioactivity, half life of radioactive element, radioactive isotopes, Induced radioactivity, GM Counter, Gas ionization detector, Scintillation counter, Quenching, Radiodating, Radioactive tracer, Autoradiography, Radioimmuno assay. Electrophoretic Methods – Principle, Types – free solution method and zone electrophoresis, Electrophoretic mobility, Factors affecting electrophoretic mobility.

Module 3

Polarography: Principles of polarographic measurements, polarograms, Description and working of dropping mercury electrode. Current and concentrations relationship. Supporting electrolyte. Limiting current, half wave potential. Factors affecting half wave potential. Migration current, Residual current and diffusion current. Modes of operation. Rapid scan polarography, differential pulse polarography, sinusoidal a.c. polarography. Applications of polarography-Identification and determination of concentration of analyte.

Module 4
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Module 5

Gas Chromatography: Principle, carrier gas, stationery phase, instrumentation, sample injection, column detectors (TCD, FID, ECD), effect of temperature on retention, qualitative and quantitative analysis. High Performance Liquid Chromatography: Principle, instrumentation, column, sample injection,detectors (absorbance, refractive index, electrochemical), mobile phase selection, ion pair chromatography.

Course Outcomes:

At the end of the course students are able

• To apply their knowledge in developing the new methods for the determination and validate the procedures.
• The appreciable knowledge will be gained by the students in the Modern Analytical Techniques and can apply the theories involved in the Analysis of various bulk drugs and their formulations.

Graduate Attributes (as per NBA):

1. Engineering Knowledge
2. Problem Analysis
3. Design/development of solutions (Partly)
4. Interpretation of data.

Question paper pattern:

• The question paper will have ten questions.
• Each full Question consisting of 20 marks
• There will be 2 full questions (with a maximum of four sub questions) from each module.
• Each full question will have sub questions covering all the topics under a module.
• The students will have to answer 5 full questions, selecting one full question from each module.

Text Books:

1. Spectrometric Identification of organic compounds, R.M. Silverstein and W.P. Webster, 6th Edition, Wiley & Sons, 1999.
2. Instrumental Methods of Analysis, H.H.Willard, L.L. Merritt and J.A. Dean and F. A. Settle, CBS Publishers, 7th Edition, 1988

Reference Books:

1. Instrumental methods of Chemical Analysis, G.W. Ewing, 5 Edition, McGraw-Hill, New York, 1988.
2. Principles of Instrumental Analysis, Skoog, D.A, S.J. Holler, T.A. Nilman, 5 Edn., Saunders college publishing, London, 1998.
3. Instrumental Methods of Chemical Analysis, Chatwal Anand, 3 Edition ,Himalaya Publishing House,1986.
4. Principles of Electroanalytical Methods, T. Riley and C. Tomilinsom, John Wiley and Sons, 2008.
5. Instrumental Methods of Chemical Analysis, K. Sharma, Goel Publishing House

For detail syllabus of all other subjects of BE Petro, 2017 scheme do visit Petro 3rd Sem syllabus for 2017 scheme.

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