Instrumental Analysis [F.C] detail syllabus for Chemical Engineering (Che), 2017 scheme is taken from VTU official website and presented for VTU students. The course code (17CH46), and for exam duration, Teaching Hr/week, Practical Hr/week, Total Marks, internal marks, theory marks, duration and credits do visit complete sem subjects post given below.
For all other che 4th sem syllabus for be 2017 scheme vtu you can visit CHE 4th Sem syllabus for BE 2017 Scheme VTU Subjects. The detail syllabus for instrumental analysis [f.c] is as follows.
Course Objectives:
The course is designed to impart the knowledge in the field of Instrumental Analysis. The various modern analytical techniques like UV-Visible, IR, NMR, Mass, GC, HPLC, different chromatographic methods and other important topics are taught to enable the students to understand and apply the principles involved in the determination of different bulk drugs and their formulation. In addition to the theoretical aspects, the basic practical knowledge relevant to the analysis is also imparted.
Module 1
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Module 2
GAS CHRO columns: pr Principles a applications, techniques. MATOGRAPHY: Introduction, fundamentals, instrumentation, paration and operation, detection, dramatization. . HPLC: nd instrumentation, solvents and columns, detection and HPTLC: Theory and principle, instrumentation, elution
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Module 3
SPECTROSCOPY: Introduction, electromagnetic spectrum, absorbance laws and limitations, instrumentation-design and working principle, chromophore concept, auxochromes, Wood-Fisher rules for calculating absorption maximum, applications of UV-Visible spectroscopy . IR spectroscopy: Basic principles-Molecular vibrations, vibrational frequency, factors influencing vibrational frequencies, sampling techniques, instrumentation, interpretation of spectra, FT-IR, theory and applications.
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Module 4
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Module 5
NMR: Theory, instrumentation, chemical shift, shielding and de-shielding effects, splitting of signals, spin-spin coupling, proton exchange reactions, coupling constant (J), nuclear over Hauser effect (NOE), 13CNMR spectra and its applications, 2D-NMR, COSY and applications
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Course Outcomes:
The appreciable knowledge will be gained by the students in the Modern Analytical Techniques and can apply the theories involved in the Analysis of various bulk drugs and their formulations. The students will also be in a position to apply their knowledge in developing the new methods for the determination and validate the procedures.
Graduate Attributes (as per NBA):
- Problem analysis.
- Design/development of solutions.
Question paper pattern:
- The question paper will have ten questions.
- Each full Question consisting of 20 marks
- There will be 2 full questions(with a maximum of four sub questions) from each module.
- Each full question will have sub questions covering all the topics under a module.
- The students will have to answer 5 full questions, selecting one full question from each module.
Text Books:
- Instrumental Methods of Chemical Analysis by B.K Sharma
- Organic Spectroscopy by Y.R Sharma
Reference Books:
- Text book of Quantitative Chemical Analysis by Vogel’s A.I.
- Organic Spectroscopy by William Kemp
For detail syllabus of all other subjects of BE Che, 2017 scheme do visit Chemical Engineering 4th Sem syllabus for 2017 scheme.
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