Instrumental Methods of Chemical Analysis detailed Syllabus for Petrochem Engineering (Petrochem), 2018 scheme has been taken from the VTUs official website and presented for the VTU students. For Course Code, Subject Names, Teaching Department, Paper Setting Board, Theory Lectures, Tutorial, Practical/Drawing, Duration in Hours, CIE Marks, Total Marks, Credits and other information do visit full semester subjects post given below.
The Syllabus PDF files can also be downloaded from the official website of the university.
For all other VTU Petrochem 3rd Sem Syllabus for BE 2018 Scheme, do visit VTU Petrochem 3rd Sem Syllabus for BE 2018 Scheme Subjects. The detailed Syllabus for instrumental methods of chemical analysis is as follows.
Course Learning Objectives:
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Module-1
General Introduction To Spectroscopy – Define Spectroscopy, Types of spectroscopy, Absorption spectrum, Emission spectra, Wave length and Wave number, Electromagnetic radiation, Visible spectrum, Stokes’s shift, Hypochromicity, transmittance. Introduction, basic principles and instrumentation – Infrared Spectroscopy, Flame Photometry, Atomic Absorption Spectroscopy and Mass Spectrometry.
Module-2
Radiochemical Techniques – Define radioactivity, half life of radioactive element, radioactive isotopes, Induced radioactivity, GM Counter, Gas ionization detector, Scintillation counter, Quenching, Radiodating, Radioactive tracer, Autoradiography, Radioimmuno assay. Electrophoretic Methods – Principle, Types – free solution method and zone electrophoresis, Electrophoretic mobility, Factors affecting electrophoretic mobility.
Module-3
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Module-4
Introduction to Chromatography: Classification – Theory – distribution coefficient, rate oftravel, retention time, retention volume, adjusted retention volume, specific retention volume, column capacity, separation number, peak capacity, shapes of chromatic peak, column efficiency, resolution, optimization of column performance, Chromatogram, Void volume. Thin Layer Chromatography: Stationary phase, mobile phase, sample application,development techniques -evaluation and documentation, advantages and disadvantages of TLC.
Module-5
Gas Chromatography: Principle, carrier gas, stationery phase, instrumentation, sample injection, column detectors (TCD, FID, ECD), effect of temperature on retention, qualitative and quantitative analysis. High Performance Liquid Chromatography: Principle, instrumentation, column, sample injection, detectors (absorbance, refractive index, electrochemical), mobile phase selection, ion pair chromatography.
Course Outcomes:
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Question Paper Pattern:
- The question paper will have ten questions.
- Each full Question consisting of 20 marks
- There will be 2 full questions (with a maximum of four sub questions) from each module.
- Each full question will have sub questions covering all the topics under a module.
- The students will have to answer 5 full questions, selecting one full question from each module.
Text Books:
- Spectrometric Identification of organic compounds, R.M. Silverstein and W.P. Webster, 6th Edition, Wiley & Sons, 1999.
- Instrumental Methods of Analysis, H.H.Willard, L.L. Merritt and J.A. Dean and F. A. Settle, CBS Publishers, 7th Edition, 1988.
Reference Books:
For the complete Syllabus, results, class timetable, and many other features kindly download the iStudy App
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For detail Syllabus of all other subjects of BE 3rd Sem Petrochem Engineering, visit (Petrochem) 3rd Sem Syllabus Subjects.
For all (CBSE & Non-CBSC) BE results, visit VTU BE all semester results direct links.