Instrumental Analysis detailed Syllabus for Chemical Engineering (CH), 2018 scheme has been taken from the VTUs official website and presented for the VTU students. For Course Code, Subject Names, Teaching Department, Paper Setting Board, Theory Lectures, Tutorial, Practical/Drawing, Duration in Hours, CIE Marks, Total Marks, Credits and other information do visit full semester subjects post given below. The Syllabus PDF files can also be downloaded from the official website of the university.
For all other VTU CH 4th Sem Syllabus for BE 2018 Scheme, do visit VTU CH 4th Sem Syllabus for BE 2018 Scheme Subjects. The detailed Syllabus for instrumental analysis is as follows.
Course Objectives:
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Module 1
CHROMATOGRAPHY: Classification of chromatographic methods based on the mechanism of separation. Column Chromatography: Adsorption and partition, theory, preparation, procedure and methods of detection. Thin Layer Chromatography: Theory, preparation, procedures, detection of compounds. Paper Chromatography: Theory, different techniques employed, filter papers used, qualitative and quantitative detection .Counter-current extraction, solid phase extraction techniques, gel filtration.
Module 2
GAS CHROMATOGRAPHY: Introduction, fundamentals, instrumentation, columns: preparation and operation, detection, dramatization. . HPLC: Principles and instrumentation, solvents and columns, detection and applications, HPTLC: Theory and principle, instrumentation, elution techniques.
Module 3
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Module 4
MASS SPECTROSCOPY: Theory, ionization techniques: electron impact ionization, chemical ionization, field ionization, fast atom bombardment, plasma desorption, fragmentation process: types of fission, resolution, GC/MS, interpretation of spectra and applications for identification and structure determination.
Module 5
NMR: Theory, instrumentation, chemical shift, shielding and de-shielding effects, splitting of signals, spinspin coupling, proton exchange reactions, coupling constant (J), nuclear over Hauser effect (NOE), 13CNMR spectra and its applications, 2D-NMR, COSY and applications.
Course Outcomes:
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Question paper pattern:
- The question paper will have ten questions.
- Each full Question consisting of 20 marks
- There will be 2 full questions (with a maximum of four sub questions) from each module.
- Each full question will have sub questions covering all the topics under a module.
- The students will have to answer 5 full questions, selecting one full question from each module
Text Books:
- Instrumental Methods of Chemical Analysis by B.K Sharma
- Organic Spectroscopy by Y.R Sharma.
Reference Books:
For the complete Syllabus, results, class timetable, and many other features kindly download the iStudy App
It is a lightweight, easy to use, no images, and no pdfs platform to make students’s lives easier..
For detail Syllabus of all other subjects of BE 4th Sem Chemical Engineering, visit (CH) 4th Sem Syllabus Subjects.
For all (CBSE & Non-CBSC) BE results, visit VTU BE all semester results direct links.