15SC06P: Chemistry Lab -1 Chemical 2nd Sem Syllabus for Diploma DTE Karnataka C15 Scheme

Chemistry Lab -1 detail DTE Kar Diploma syllabus for Chemical Engineering (CH), C15 scheme is extracted from DTE Karnataka official website and presented for diploma students. The course code (15SC06P), and for exam duration, Teaching Hr/week, Practical Hr/week, Total Marks, internal marks, theory marks, duration and credits do visit complete sem subjects post given below. The syllabus PDFs can be downloaded from official website.

For all other chemical 2nd sem syllabus for diploma c15 scheme dte karnataka you can visit Chemical 2nd Sem Syllabus for Diploma C15 Scheme DTE Karnataka Subjects. The detail syllabus for chemistry lab -1 is as follows.

Pre-requisites:

Knowledge: Basic concepts of Chemistry in Secondary Education.

Course Objectives:

To provide practical knowledge about the Basics of preparation of chemical solutions and qualitative and quantitative analysis of chemical compounds.

Tutorial: 01Hr/Experiment.

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Conducting of an experiment:

2Hrs/Experiment

List of Graded Exercises:

QUALITATIVE ANALYSIS: (18 HRS)

Semi micro-analysis of Anions of Inorganic salts containing: Carbonate, bicarbonate, Chloride, Nitrate and Sulphate radicals.

QUANTITATIVE ANALYSIS: (60 HRS)

Volumetric Analysis by Titrimetric Method:-

Volumetric Analysis – Titration – Standard solutions , concentration of solutions- normal, molar and molal solutions – decinormal, decimolar and decimolal solutions – indicators -acidbase indicators and redox indicators-selection of indicators -endpoint of titration -neutralization and redox reactions.

I. Preparation of standard solution of Known concentration: 18 Hrs

1. Preparation of 0.1N Oxalic acid
2. Preparation of 0.1N sodium Carbonate solution
3. Preparation of 0.1N Potassium Dichromate solution
4. Preparation of 0.1N NaOH Solution
5. Preparation of 0.1N HCl solution
6. Preparation of 0.1N Sulphuricacid
7. Preparation of 0.1N Mohr’s salt solution.
8. Preparation of 0.1N Potassium permanganate solution.

II. Standardization of solutions:- 18 Hrs

1. Determination of normalityof given NaOH solution using standard decinormal oxalic acid solution.
2. Determination of normality of given HCl solution using decinormal sodium Carbonate solution.
3. Determination of normality of NaOH solution using decinormalHCl solution.
4. Determination of normality of given potassium permanganate solution using decinormal oxalic acid solution.
5. Determination of normality of given Mohr’s salt solution using decinormal Potassium dichromate solution (Internal Indicator).

III. Estimation of amount of substance in 250cm3 of its solution by link solution. 24Hrs

1. Estimation of mass of HCl in 250 cm3of its solution using standardNaOH solution which is standardized by decinormal oxalic acid solution.
2. Estimation of mass of NaOHin 250cm3 of its solution using standard HCl solution which is standardized by decinormal Na2CO3.
3. Estimation of mass of oxalic acid in 250cm3of its solution using standard NaOH solution which is standardized by decinormalHCl solution.
4. Estimation of mass of Mohr’s salt in 250cm3 of its solution using standard KMnO4 solution, which is standardized by decinormal oxalic acid solution
5. Estimation of mass of KMnO4in 250cm3of its solution using standard Mohr’s salt solution, which is standardized by decinormal K2Cr2O7 Solution.

Course Outcomes:

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Reference Books:

1. Vogel’s Inorganic Qualitative and Quantitative Analysis.
2. Practical chemistry By O.P.Pande.& others.
3. Qualitative and quantitative analysis by Alex

Course Delivery:

The Course will be delivered through lectures, classroom interaction, group discussion, graded exercises, demonstrations and assignments.

Conduction of experiments: 2 Hrs/Experiment.

For complete syllabus and results, class timetable and more pls download iStudy Syllabus App. Its a light weight, easy to use, no images, no pdfs platform to make students life easier.

Course Outcomes:

1. CO1 Identify chemical sample compound.
2. CO2 Prepare the standard solutions.
3. CO3 Standardize the given unknown concentration solution.
4. CO4 Estimate the mass of the chemical substance in the given sample of solution.
5. C05 Relate the answers to the oral questions.

LIST OF EQUPIMENT REQUIRED

1. BURETTE 50ml 50
2. PIPETTE 10ml 50
3. PIPETTE 25ml 50
4. CONICAL FLASK 250ml 50
5. VOLUMETRIC FLASK 100ml 30
6. VOLUMETRIC FLASK 250ml 30
7. VOLUMETRIC FLASK 500ml 10
8. VOLUMETRIC FLASK 1000ml 05
9. BEAKER 400ml 30
10. BEAKER 1000ml 20
11. BEAKER 250ml 30
12. REAGENT BOTTLE 500ml 50
13. INDICATOR BOTTLE 100ml 05
14. BURETTE STAND WITH CLAMP STEEL 20
15. PIPETTE STAND PLASTIC 05
16. TEST TUBE 20ml 50
17. TEST TUBE HOLDER 20
18. TEST TUBE BRUSH 20
19. TEST TUBE STAND PLASTIC 10

For detail syllabus of all other subjects of BE Chemical, C15 scheme do visit Chemical 2nd Sem syllabus for C15 scheme.

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