15EI63B: Analytical Instrumentation Instrumentation 6th Sem Syllabus for Diploma DTE Karnataka C15 Scheme

Analytical Instrumentation detail syllabus for Electronics Instrumentation And Control Engineering (65), C15 scheme is taken from DTE Karnataka official website and presented for diploma students. The course code (15EI63B), and for exam duration, Teaching Hr/week, Practical Hr/week, Total Marks, internal marks, theory marks, duration and credits do visit complete sem subjects post given below.

For all other instrumentation 6th sem syllabus for diploma c15 scheme dte karnataka you can visit Instrumentation 6th Sem Syllabus for Diploma C15 Scheme DTE Karnataka Subjects. For all other Elective subjects do refer to Elective. The detail syllabus for analytical instrumentation is as follows.

Pre-requisites:

Applied Science , Basics of Electrical & Electronic Engg., Industrial Instrumentation , Electronic Measurement

Course Objectives:

• To understand the analytical instrumental analysis.
• To understand basic analytical processes and sampling procedures
• To understand the basic principles of spectroscopy
• To understand the basic concept of refractometers

Course Outcomes:

For complete syllabus and results, class timetable and more pls download iStudy. Its a light weight, easy to use, no images, no pdfs platform to make students life easier.

UNIT I Fundamentals of Analytical Instruments 05 Hours

Introduction, Elements of an Analytical Instruments, Applications of chemical composition measurement in industries, classification of analytical instruments based on properties

UNIT II Analysis using Mechanical and Thermal properties 10 Hours

Viscosity measurement techniques:- terminologies, Saybolt viscometer, Density and specific gravity measurement techniques:- pressure head type, densitometer, Displacer type densitometer, Float type densitometer, Buoyancy effect type densitometer, Thermal conductivity analysis:- Principle, Dual hot wire thermal conductivity cell.

UNIT III Analysis using Electrical properties 07 Hours

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UNIT IV Oxygen Analysers 08 Hours

Oxygen analyser: – Paramagnetic oxygen analyser:- dumb bell type, wind type, Heat of reaction analyser, Dissolved oxygen analyser, Polarography:- Electrodes Dropping mercury electrode, Saturated calomel electrode

UNIT V Analysis using radiation properties 12 Hours

Electromagnetic radiation:- electromagnetic spectrum, Interaction of radiation with matter, Laws relating to absorption of radiation:- Lamberts law, Beers law, Beer-Lamberts law,
Absorption instruments:- colorimeter (photometer), spectrophotometer, X-ray technique of analysis by diffraction, Nuclear Magnetic resonance:- Principle, block diagram

UNIT VI Analysis using miscellaneous properties 10 Hours

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Reference Books:

1. Hand book of Analytical Instruments R.S.Khandpur Tata McGraw Hill, New Delhi
2. Analytical Instrumentation BelaG.Lipkat Chilton bookcompany
3. Principle of industrial instrumentation D.Patranabis Tata McGraw Hill, New Delhi
4. Process instrumentation and control A.P.Kulkarni NiraliPrakashan,pune
5. Instrumental methods of analysis H.H.Willard CBS Publishers & Distributers

SUGGESTED STUDENT ACTIVITY:-

The student should be able to perform any one activity from each example

Example:-1

• The student has to Study the different types of Analytical Instruments by doing a survey and then submit a handwritten report. Documents have to be maintained as a record.
• Take Quiz tests / assignments in topics based on Analytical Instrumentation . Documents have to be maintained as a record.
• Do a power point presentation on any type of Analytical instrument . Documents have to be maintained as a record.
• Visit YouTube sites relevant to topics on Analytical Instrumentation . Listen to the lectures and submit a handwritten report

Example:-2

• Do a market survey of Analytical Instruments based on Mechanical / Electrical / Radiation properties and submit a report
• Collect Data on pH of different solutions and submit a handwritten report.
• Submit a report on where Gas Chromatography / Refractrometry can be used.

Course Delivery:

• The course will be delivered through lectures and Power point presentations/ Video

Model Question Paper:

PART-A

1. Draw and explain elements of an analytical instrument. 5 marks
2. Define density and specific gravity. 5 marks
3. Enlist types of density measurement techniques 5 marks
4. Define the following terms:- conductivity, conductance 5 marks
5. Explain the working principle of conductivity cell 5 marks
6. State Beer- Lambert’s law 5 marks
7. State the limitation of refractometer 5 marks
8. Explain theory of operation of refractometer. 5 marks
9. List applications of Gas chromatograph 5 marks

PART B

1. Describe working principle, construction with schematic diagram of density and specific gravity measurement techniques 10 marks
2. Draw and explain the dual hotwire thermal conductivity cell 10 marks
3. Draw and explain null method of conductance measurement 10 marks
4. Explain principle, working and construction of Dumbell type paramagnetic oxygen analyser 10 Marks
5. Illustrate the application of combination electrode for pH measurement10 marks
6. Explain block diagram of NMR spectrometer 10 marks
7. Enlist the application of X-ray absorption spectrometer 10 marks
8. Describe single pass refractometer with neat sketch. 10 marks
9. Draw and explain block diagram of a Gas chromatograph 10 marks
10. Explain the basic parts of Gas chromatograph andListits applications 10 marks

Model Question Paper:

(CIE)

1. Give the applications of chemical composition analysis

Or Draw and explain elements of an analytical instruments

2. Classify analytical instruments based on properties that are utilised in the analysis
3. Explain the principle of Saybolt’s voltmeter

Or Enlist the types of density measurement techniques

4. List different techniques of filling gas to thermal conductivity cell

Software Learning Sites for Analytical Instrumentation

1. Gas chromatography
1. http://www.sigmaaldrich.com/analytical- chromatography HYPERLINK “
2. http://www.sigmaaldrich.com/analytical-chromatography”HYPERLINK “
3. http://www.slideshare.net/banuman35/applic ations-of-gas-%20chromatography-“HYPERLINK “
4. http://www.sigmaaldrich.com/analytical-chromatography”
5. http://www.slideshare.net/b anuman35/applications-of-gas-chromatography-HYPERLINK “
6. http://www.sigmaaldrich.com/analytical-chromatography”HYPERLINK “
7. http://www.slideshare.net/banuman35/applic ations-of-gas-chromatography-applications-of-gc-by-pravisankar”HYPERLINK “
8. http://www.sigmaaldrich.com/analytical-chromatography”applications-of-gc-by-pravisankar
2. Refractometer
1. http://www.intercomir.it/laboratorio/rifrappl_ en.html HYPERLINK “
2. http://www.intercomir.it/laboratorio/rifrappl _en.html”
3. http://www.misco.com/refractomet er-support/refractometer-forum/refractometerHYPERLINK “
4. http://www.intercomir.it/laboratorio/rifr appl_en.html”-HYPERLINK “
5. http://www.intercomir.it/laboratorio/rifr appl_en.html”HYPERLINKHYPERLINK “
6. http://www.intercomir.it/laboratorio/rifr appl_en.html” “
7. http://www.misco.com/refractometer-support/refractometer-forum/refractometer-applications”HYPERLINK “
8. http://www.intercomir.it/laboratorio/rifr appl_en.html”applications
3. Spectrophotometer
1. http://www.slideshare.net/suniu/spectroph otometry-16091660pHmeter
2. http://www.wikihow.com/Calibrate-and-Use-a-pH-Meter

Note:- Similar sites can be re ferred for other topics

For detail syllabus of all other subjects of BE Instrumentation, C15 regulation do visit Instrumentation 6 syllabus for C15 Regulation.

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