Mass Transfer Operations-II detail BTEUP syllabus for Chemical Engineering, effective from 2019-2020, is collected from BTEUP 2017 Syllabus official website and presented for diploma students. PDF download is possible from official site but you can download the istudy mobile app for syllabus on mobile. The course details such as exam duration, Teaching Hr/week, Practical Hr/week, Total Marks, internal marks, theory marks, duration and credits do visit complete sem subjects post given below. The syllabus PDFs can be downloaded from official website.
For all other bteup syllabus 5th sem chemical eng 2019-2020 you can visit BTEUP Syllabus 5th Sem Chemical Eng 2019-2020 Subjects. The detail syllabus for mass transfer operations-ii is as follows.
Rationale:
In this subject, the basic concepts of mass transfer are covered to enable the students to understand working of various mass transfer equipment like distillation columns, crystallizers and extractors which are used in industries.
Learning Outcomes:
After the completion of this course, the students will be able to:
- Understand the concept of distillation.
- Analyze problems involving calculation of trays required for desired separation in binary distillation column
- Understand and evaluate the performance of various mass transfer operations like extraction, leaching, adsorption, crystallization and membrane separation
1. Distillation (25 periods)
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2. Extraction (12 periods)
Definition and application of extraction, (final expression and physical meaning of terms therein, no derivation) equipment: mixer settler, spray and packed extraction towers, perforated plate extraction tower, agitated tower extractor.
3. Leaching (08 periods)
Definition and application of leaching, equipment: leaching through stationary solid beds, moving beds, ideal stages in counter current leaching.
4. Adsorption (10 periods)
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5. Membrane Separation and Crystallization (15 periods)
- Introduction to Membrane Separation, Types of Membrane, Membrane Separation Processes, Brief Introduction: reverse osmosis, microfiltration, ultra filtration, nano filtration, dialysis.
- Concept of crystallization, saturation and super saturation and solubility curve, mechanism of crystallization/crystal formation, method of super saturation – Miers super saturation theory.
- Classification of crystallizers – construction and working of agitated tank crystallizer, draft tube baffle crystallizer, Swenson walker crystallizer, vacuum crystallizer.
List of Experiments:
- To find out diffusion coefficient in liquid
- To find out diffusion coefficient in solid
- To study on packed bed absorption tower
- To study time of batch drying in tray tower
- To find out overall man transfer coefficient welted wall column
- To separate given solution mixture with the help of a sieve plate distillation
- To draw calibration curve for a given mixture using refractive index and to find out the unknown concentration from this calibration curve using abbes refretometer
- To study and determine the efficiency of solid-liquid extraction
- To study the performance of crystallizer
- To separate a mixture of two liquid using liquid extraction and calculate separation efficiency.
- To verify Relish’s equation using batch distillation set-up
Means of Assessment:
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Instructional Strategy:
Field visit will make the students familiar with different types of column (packed/tray), different types of packing used in the column, different types of extractors and membrane separation techniques. This will also make the students aware of auxiliary equipment/model/ supports for different equipment. Emphasis should also be given to problem solving and practices especially for distillation column and extraction.
Text Books:
- Mass Transfer Operations by Treybal, Kogakusha Publication
- Introduction to Chemical Engineering by Badger and Banchero; McGraw Hill Publication
- Unit Operations of Chemical Engineering by Mc Cabe and Smith; McGraw Hill Publication
- Mass Transfer by Sherwood Pigford and Wilke; McGraw Hill Publication
- Chemical Engineering Handbook by Perry and Chilton; McGraw Hill Publication
- Mass Transfer by K.A Gavhane, Nirali Publication
For detail syllabus of all other subjects of BE Chemical Eng, effective from 2019-2020 do visit Chemical Eng 5th Sem BTEUP syllabus for 2019-2020.
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