Analytical Instrumentation detail syllabus for Electronics & Communication Engineering (ECE), 2019-20 scheme is taken from AKTU official website and presented for AKTU students. The course code (REC081), and for exam duration, Teaching Hr/Week, Practical Hr/Week, Total Marks, internal marks, theory marks, and credits do visit complete sem subjects post given below.
For all other ece 8th sem syllabus for b.tech 2019-20 scheme aktu you can visit ECE 8th Sem syllabus for B.Tech 2019-20 Scheme AKTU Subjects. For all other Departmental Elective-V subjects do refer to Departmental Elective-V. The detail syllabus for analytical instrumentation is as follows.
Unit I
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Unit II
Infrared Spectroscopy, Basic Components of IR Spectrophotometers, Type of Infrared Spectrophotometers, Sample Handling Techniques
Unit III
Flame photometers: principle, constructional details of flame photometers, types of flame photometers, types of flame photometers, clinical flame photometers, accessories for flame photometer, expression for concentration, interferences in flame photometry, procedure for determinations. Atomic Absorption Spectrometers: Atomic Absorption Spectroscopy, Atomic Absorption Instrumentation, Sources of interferences, meter scale.
Unit IV
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Unit V
Nuclear Magnetic Resonance (NMR) Spectroscopy, Principle of NMR, types of NMR spectrometers, constructional details of NMR spectrometer, variation T-60A NMR spectrometer, sensitivity enhancement for analytical NMR-spectroscopy, Fourier transform NMR spectroscopy.
Course Objectives:
- Understand UV-Visible Spectroscopy.
- Understand Infrared Spectroscopy.
- Learn working of flame photometers.
- Interpret working of mass Spectrometers.
- Be aware of Nuclear Magnetic Resonance (NMR) Spectroscopy.
Course Outcomes:
- Understand the Electromagnetic Radiation, Laws relating to absorption radiation, Absorption Instruments, Ultraviolet and visible absorption spectroscopy, Calorimeters.
- Design basic components of IR Spectrophotometers, Type of Infrared Spectrophotometers, Sample Handling Techniques.
- Learnprinciple, constructional details of flame photometers, types of flame photometers, types of flame photometers.
- Be aware of Basic Mass Spectrometer, Principle of operation, Type of Mass Spectrometers, components of Mass Spectrometers, inductively coupled plasma-mass spectrometer.
- Understand the Principle of NMR, types of NMR spectrometers, constructional details of NMR spectrometer
Reference Books:
- DA Skoog, Principles of Instrumental Analysis, 6th Ed. Cengage
- R. S. Kandpur, Handbook Of Analytical Instruments, Mc Graw Hill 3rdEdition,
- Willard, Merritt, Dean and Settle, Instrumental Methods of Analysis, 7thEdition, CBS Publishers.
For detail syllabus of all other subjects of B.Tech Ece, 2019-20 regulation do visit Ece 8th Sem syllabus for 2019-20 Regulation.
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