ISC404: Analytical Instrumentation Syllabus for IS 4th Sem 2017 Pattern Mumbai University

Analytical Instrumentation detailed syllabus scheme for Instrumentation Engineering (IS), 2017 regulation has been taken from the University of Mumbai official website and presented for the Bachelor of Engineering students. For Course Code, Course Title, Test 1, Test 2, Avg, End Sem Exam, Team Work, Practical, Oral, Total, and other information, do visit full semester subjects post given below.

For all other Mumbai University Instrumentation Engineering 4th Sem Syllabus 2017 Pattern, do visit IS 4th Sem 2017 Pattern Scheme. The detailed syllabus scheme for analytical instrumentation is as follows.

Analytical Instrumentation Syllabus for Instrumentation Engineering SE 4th Sem 2017 Pattern Mumbai University

Course Objectives:

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Course Outcomes:

The students will be able to:

1. Define and explain various fundamentals of spectroscopy, qualitative and quantitative analysis.
2. Discuss the terms, principle, instrumentation, operation and applications of Molecular spectroscopic techniques.
3. Differentiate between principle, instrumentation and operation of Atomic absorption and emission Spectroscopy.
4. Explain the various Separation techniques and its instrumentation.
5. Describe the principle and working of various Radiation detectors.
6. Discuss the principle and working of various Gas analyzers.

Prerequisites:

Knowledge of sensors and analog electronic circuits.

Module 1

Introduction: Introduction to analytical Instrumentation. Compare classical analytical techniques with instrumental techniques. Fundamentals of Spectroscopy: Nature of Electromagnetic Radiation, Electromagnetic spectrum, Beer Lamberts Law statement and derivation. Deviations from Beers law. Numerical on EMR and laws of photometry. Interaction of radiation with matter. Instrumentation of spectroscopic analytical system – Radiation sources, Wavelength selectors, Detectors, signal processors and readout modules. 06 CO1

Module 2

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Module 3

Atomic Spectroscopy: Atomic Energy levels, Atomic absorption spectrometers- components, working and absorption spectra. Atomic Emission spectrometers – components, working and emission spectra, comparison between AAS and AES. 03 CO3

Module 4

Separation Science: Chromatography: Fundamentals of chromatographic Separations, Classification, Gas chromatographic system with components, factors affecting separation, applications. Analysis of Gas Chromatogram. HPLC – Its principle and instrumentation. Mass Spectrometers: Basic principle, components and types of mass spectrometers, sample handling techniques for liquids and solids, resolution and numerical problems based on resolution. Interfacing Gas Chromatography and Mass spectrometry (GCMS). 09 CO4

Module 5

Radio Chemical Instrumentation: Basics of Radioactivity, properties of radiations (a, P, y). Halflife period and numerical problems based on half-life period. Radiation detectors – Ionization chamber, Proportional counter, Geiger Muller counter, Scintillation detector, Semiconductor detectors, Pulse height analyzers. 05 CO5

Module 6

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Internal Assessment:

Internal Assessment consists of two tests out of which, one should be compulsory class test (on minimum 02 Modules) and the other is either a class test or assignment on live problems or course project. End Semester Theory Examination:

1. Question paper will comprise of 6 questions, each carrying 20 Marks.
2. Total 4 questions need to be solved.
3. Question No. 1 will be compulsory and based on entire syllabus wherein sub questions will be of 4 to 5 marks.
4. Remaining questions will be mixed in nature.
5. In question paper weightage of each module will be proportional to the number of respective lecture hours as mentioned in the syllabus.

Text Books:

1. Willard, Merritt, Dean, Settle, Instrumental Methods of Analysis, CBS Publishers & Distributors, New Delhi, 7th Edition.
2. Khandpur R. S., Handbook of Analytical Instruments, Tata McGraw-Hill Publications, 3rd Edition.

Reference Books:

1. Skoog, Holler, Niemen, Thomson Principles of Instrumental Analysis, Books-Cole Publications, 5th Edition.
2. Ewing Galen W., Instrumental Methods of Chemical Analysis, McGraw-Hill Book Company, 5th Edition.
3. Braun Robert D., Introduction to Instrumental Analysis, McGraw-Hill Book Company.
4. Sherman R.E., Analytical Instrumentation, ISA Publication.
5. B.R.Bairi, Balvindersingh, N.C.Rathod, P.V.Narurkar Handbook nuclear medical Instruments, McGraw-Hill Book Company.

For detail syllabus of all other subjects of Instrumentation Engineering (IS) 4th Sem 2017 regulation, visit IS 4th Sem Subjects syllabus for 2017 regulation.