Instrumental Methods of Analysis – Theory detailed Syllabus Scheme for Bachelor of Pharmacy (B.Pharm), 2019 regulation has been taken from the University of Mumbai official website and presented for the Pharmacy students. For Course Code, Subject Name, Continuous Mode, SE Marks, SE Duration, Total, Marks, Duration in Hours, Total Marks, and other information, do visit full semester subjects post given below.
For all other Mumbai University B.Pharm 7th Sem Syllabus 2019 Pattern, do visit B.Pharm 7th Sem 2019 Pattern Scheme. The detailed syllabus scheme for instrumental methods of analysis – theory is as follows.
BP701T: Instrumental Methods of Analysis – Theory Syllabus for B.Pharm 7th Sem 2019 Pattern Mumbai University
Scope:
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Objectives
Upon completion of the course the student shall be able to:
- Understand the interaction of matter with electromagnetic radiations and its applications in drug analysis
- Understand the chromatographic separation and analysis of drugs.
- Perform quantitative & qualitative analysis of drugs using various analytical instruments.
UNIT -I-UV Visible spectroscopy 10
- Electronic transitions, chromophores, auxochromes, spectral shifts, solvent effect on absorption spectra, Beer and Lamberts law, Derivation and deviations. 3
- Instrumentation – Sources of radiation, wavelength selectors, sample cells, detectors-Photo tube, Photomultiplier tube, Photo voltaic cell, Silicon Photodiode. 2
- Applications – Spectrophotometric titrations, Single component and multi component analysis 2
- Fluorimetry Theory, Concepts of singlet, doublet and triplet electronic states, internal and external conversions, factors affecting fluorescence, quenching, instrumentation and applications 3
UNIT -II -IR spectroscopy 10
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UNIT -III Introduction to chromatography 10
- Adsorption and partition column chromatography- Methodology, advantages, disadvantages and applications. 4
- Thin layer chromatography- Introduction, Principle, Methodology, Rf values, advantages, disadvantages and applications. 2
- Paper chromatography-Introduction, methodology, development advantages, disadvantages and applications 2
- Electrophoresis-Introduction, factors affecting electrophoretic mobility, Techniques of paper, gel, capillary electrophoresis, applications 2
UNIT -IV 8
- Gas chromatography – Introduction, theory, instrumentation, derivatization,temperature programming, advantages, disadvantages and applications 4
- High performance liquid chromatography (HPLC)-Introduction, theory,instrumentation, advantages and applications. 4
UNIT -V 7
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Reference Books:
- Instrumental Methods of Chemical Analysis by B.K Sharma
- Organic spectroscopy by Y.R Sharma
- Text book of Pharmaceutical Analysis by Kenneth A. Connors
- Vogels Text book of Quantitative Chemical Analysis by A.I. Vogel
- Practical Pharmaceutical Chemistry by A.H. Beckett and J.B. Stenlake
- Organic Chemistry by I. L. Finar
- Organic spectroscopy by William Kemp
- Quantitative Analysis of Drugs by D. C. Garrett
- Quantitative Analysis of Drugs in Pharmaceutical Formulations by P. D. Sethi
- Spectrophotometric identification of Organic Compounds by Silverstein
For detail syllabus of all other subjects of Bachelor of Pharmacy (B.Pharm), 2019 regulation do visit B.Pharm 7th Sem Subjects syllabus for 2019 regulation.