315354: Analytical Instrumentation Syllabus for Instrumentation 5th Sem K Scheme MSBTE PDF

Analytical Instrumentation detailed Syllabus for Instrumentation (IS), K scheme PDF has been taken from the MSBTE official website and presented for the diploma students. For Subject Code, Subject Name, Lectures, Tutorial, Practical/Drawing, Credits, Theory (Max & Min) Marks, Practical (Max & Min) Marks, Total Marks, and other information, do visit full semester subjects post given below.

For all other MSBTE Instrumentation 5th Sem K Scheme Syllabus PDF, do visit MSBTE Instrumentation 5th Sem K Scheme Syllabus PDF Subjects. The detailed Syllabus for analytical instrumentation is as follows.

Rationale

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Course Outcomes:

Students will be able to achieve & demonstrate the following COs on completion of course based learning

1. Select the relevant analytical instruments for given sample/product.
2. Illustrate the various techniques and methods of different types of Spectrometer and Nuclear magnetic resonance (NMR).
3. Select appropriate Chromatography techniques for Gas Chromatography (GC) and Liquid Chromatography (LC).
4. Maintain analytical instruments used to analyze industrial gases.
5. Maintain analytical instruments to monitor environment pollutants.

Unit I

Basics of Analytical Instrumentation 1.1 Analytical Instrument: Block diagram, Functions of each Block 1.2 Properties of Analytes and techniques used in Analytical Instrument 1.3 Classification of Analytical Instruments: Spectral, Electro-analytical, Separation method (Introduction to each method) 1.4 Elements of Analytical Instruments: Radiation Sources- Incandescent lamp, Discharge lamp, LASER; Filters- Optical filters, Absorption Filters; Monochromators -Prism, Grating

Suggested Learning Pedagogie
Lecture Using Chalk-Board Presentations

Unit II

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Unit III

Chromatography 3.1 Chromatography – Principle, Classification (Based on – Mechanism of separation, Type of mobile Phases, Shape of Chromatography Bed) 3.2 Gas Chromatography (GC): Principle, basic parts of GC and applications 3.3 Liquid Chromatography (LC): Principle, working and applications of LC and High performance liquid chromatography (HPLC) 3.4 Mass Spectrometer : Principle, working, applications (GCMS,LCMS) and types of Mass Analyzers in Mass Spectrometry (MS) – Time of flight type, Magnetic Sector Mass Analyzer

Suggested Learning Pedagogie
Lecture Using Chalk-Board Video Demonstrations Presentations Site/Industry Visit Flipped Classroom Collaborative learning

Unit IV

1. 4.2 Blood gas Analyzer- Block diagram, Function of each blocks, measurement of pH, pCO2,pO2 4.3 Infrared gas Analyzer: Principle, Block Diagram, Working, Applications 4.4 Thermal Conductivity Analyzer: Principle, Block Diagram, Working, Applications 4.5 Paramagnetic Oxygen Analyzer – Principle, Block Diagram, Working, Applications 4.6 pH Measurement Methods – Indicator methods i. Metal-electrode methods (Hydrogen-electrode method, Quinhydrone-electrode method and Antimony-electrode method) ii. Glass-electrode methods iii. Semiconductor sensor methods) 4.7 Sample Handling system : Basics and process, Standard operating process

Suggested Learning Pedagogie
Lecture Using Chalk-Board Video Demonstrations Presentations Site/Industry Visit Flipped Classroom Collaborative learning

Unit V

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List of Experiments:

1. *Identification of elements of Analytical Instruments
2. *Measurement of absorbance and transmittance using Colorimeter
3. Measurement of absorbance and transmittance using Spectrophotometer
4. *Measurement of content using Flame photometer
5. Demonstration of NMR spectroscopy (Video/annimation)
6. *Separation of contents using Gas chromatography
7. Demonstration of separation of contents using High performance liquid chromatography (Video/annimation)
8. *Demonstration of GCMS/LCMS for separation of sample contents (Video/annimation)
9. *Measurement of pH value using pH meter
10. Analysis of gas sample using IR gas analyzer
11. Analysis of gas sample using Thermal conductivity gas analyzer
12. *Measurement of concentration of oxygen
13. (Video/annimation)
14. *Measurement of conductivity using conductivity meter
15. Demonstration of O3 gas detection using Ozone detector (Video/annimation)
16. Demonstration of Nitrogen Oxides measurement using Chemiluminescence analyzer

Self Learning

Micro Project

• Measure pH of given water samples (drinking water, sewage water, Sea water etc.) with the help of pH testing strips and prepare a report on it.
• Build an analogous model showing internal construction of Gas Chromatography/ Liquid Chromatography/ Colorimeter/ Spectrophotometer/ Flame Photometer.
• Verification of Beer Lambert’s Law using virtual lab and prepare a report.
• Build a Prism Monochromators and prepare a report on it.

Visit

• Visit pathology laboratories to observe different analysis carried out there and prepare a report on it.
• Visit a PUC (Pollution under control) center and observe the measurement of pollutants concentration in environment and prepare a report on it.
• Visit a Chemical industry to observe operation of Analytical instruments and prepare a report on it.
• Visit a National Chemical Laboratory, Pune to observe operation of Analytical instruments and prepare a report on it.

Assignment

• Prepare a report based on internet survey of advanced analytical equipment’s – Bilirubin testing equipment, Dairy testing solutions, Clinical Osmometers, Anaerobic jar systems.
• Prepare a report on safety precautions to be followed to operate various analytical equipment.
• Prepare a case study which illustrates the calibration problem and solution of Analytical Instrument.

Laboratory Equipment

For the complete Syllabus, results, class timetable, and many other features kindly download the iStudy App
It is a lightweight, easy to use, no images, and no pdfs platform to make students’s lives easier.
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Learning Materials

1. Khandpur R.S. Handbook of Analytical Instruments McGraw Hill Education, ISBN- 13: 978-9339221355 ISBN -10: 9789339221355
2. Liptak B. G. Analytical Instrumentation CRC Press, 2018, ISBN:9781351466516
3. Willard Merritt Dean Settle Instrumental Methods of Analysis CBS Publishers ,ISBN-13: 978-8123909431 ISBN-10 : 8123909438
4. Ewing, Galen W. Instrumental Methods of Chemical Analysis McGraw-Hill Inc.US; 3rd edition,ISBN-13:978-0070198517 ISBN-10:0070198519
5. Braun Robert D. Introduction to Instrumental Analysis BSP BOOKS, ISBN-13 978-9381075920
6. Skoog Holler & Crouch Principles of Instrumental Analysis Cengage India Private Limited, ISBN-13 9789353506193 ISBN-10 9353506190

Learning Websites

1. https://nptel.ac.in/courses/104105084 NOC: Analytical chemistry, IIT Kharagpur
2. https://archive.nptel.ac.in/courses/104/108/104108078/ Principles and Applications of NMR Spectroscopy.
3. https://mas-iiith.vlabs.ac.in/List%20of%20experiments.html Verification of Beer Lambert’s Law.
4. https://vlab.amrita.edu/index.php?sub=2&brch=190 Spectrophotometry
5. https://ccnsb06-iiith.vlabs.ac.in/List%20of%20experiments.ht ml NMR spectroscopy, IR spectroscopy, Mass spectroscopy.
6. https://photon-science.desy.de/facilities/petra_iii/e308646/ e310494/index_eng.html Virtual Laboratory for Instrumental Analysis (VIA).
7. https://nptel.ac.in/courses/103108100 Modern Instrumental Methods of Analysis, IISc Bangalore
8. http://www.digimat.in/nptel/courses/video/102107028/L16.html Low-pressure liquid chromatography (LPLC) and high performance liquid chromatography (HPLC)
9. https://www.youtube.com/watch?v=64Hl_TPrO94 Introduction to Chromatography II by NPTEL IIT KHARAGPUR
10. http://acl.digimat.in/nptel/courses/video/103108139/L21.html IR Gas Analysers
11. https://archive.nptel.ac.in/courses/103/106/103106162/ Environmental quality monitoring and analysis

For detail Syllabus of all other subjects of Instrumentation, K scheme do visit Instrumentation 5th Sem Syllabus for K scheme.

For all Instrumentation results, visit MSBTE Instrumentation all semester results direct links.