Analytical Instrumentation detailed Syllabus for Instrumentation (IS), I – scheme has been taken from the MSBTE official website and presented for the diploma students. For Subject Code, Subject Name, Lectures, Tutorial, Practical/Drawing, Credits, Theory (Max & Min) Marks, Practical (Max & Min) Marks, Total Marks, and other information, do visit full semester subjects post given below.
For all the other Instrumentation IS syllabus for 5th Sem, do visit Diploma in Instrumentation 5th Sem I – Scheme. For all the Instrumentation Elective-I subjects refer to Instrumentation Elective-I Scheme. The detail syllabus for analytical instrumentation is as follows.
Rationale:
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Competency:
The aim of this course is to help the student to attain the following industry identified competency through various teaching learning experiences:
- Maintain industrial analytical instruments.
Course Outcomes:
The theory, practical experiences and relevant soft skills associated with this course are to be taught and implemented, so that the student demonstrates the following industry oriented COs associated with the above mentioned competency:
- Select the relevant analytical instruments for various applications.
- Maintain the instruments based on absorption spectroscopy.
- Maintain the instruments based on separation techniques.
- Use relevant analytical instrument for specified industrial gases.
- Maintain analytical instruments to monitor environment pollutants.
Suggested Exercises:
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Instruments Required:
The major equipment with broad specification mentioned here will usher in uniformity in conduct of experiments, as well as aid to procure equipment by authorities concerned.
Equipment Name with Broad Specifications
- Single beam filter Colorimeter: wavelength range- 340-900nm
- Double beam Spectrophotometer: wavelength range- 190-2700nm
- Flame photometer: Ranges Na: 1-lOOppm, K: 1-lOOppm, Li: 1-JOOppm, Ca: 15-lOOppm, Ba: 50-1000ppm.
- Gas chromatography: Retention time repeatability – < 0 008% or < 0 0008 min Area repeatability – < 1% RSD, using 2ng tetradecane, Must support simultaneously: – two inlets – three detectors
- High performance liquid chromatography: The flow rate should be within a range from 0 001 to 20 ml/min, Flow Accuracy: 1 0% or better
- Mass spectrometer: Mass range (m/z) 10 – 1250 with unit mass resolution, Power 100-240 VAC, 50/60 Hz
- pH meter, Range 0-14 Accuracy-0 1% of range ,Temp compensation-0 to 100 C
- 1R gas analyzer:Range:C02-20%,CO-30%,H2-30%,02-5%,CH4-l 0%
- Thermal conductivity gas analyzer: Components:H2, He ,Ar,CH4 Output signal:4-20 mA DC, 0-1 V DC, or 0-10 mV DC
- Paramagnetic oxygen analyzer: Measurement range : Auto ranging from 0 01 to 100% Oxygen
- Conductivity meter:SO2-0 … 20 ppm O3-O … 1 ppm
Unit 1
Introduction to analytical instrumentation
Total Teaching Hours – 06
Distribution of Theory Marks
R Level – 02
U Level – 04
A Level – —
Total Marks – 06
Unit Outcomes (UOs) (in cognitive domain)
- Describe function of given blocks of the block diagram of the Analytical Instrument.
- Categorize the given analytical instrument based on property of analyte.
- Classify the given analytical instruments based on working principle.
- Use various elements in given analytical instruments.
Topics and Sub-topics
- Analytical Instrument: Block diagram, Explanation.
- Properties of Analytes and techniques used in Analytical Instrument
- Classification: Spectral, Electro-analytical, Separation method(Introduction to each method)
- Elements of Analytical Instruments: Radiation Sources: Incandescent lamp, Discharge lamp LASER; Optical filters; Absorption Filters, Monochromators -Prism, Grating
Unit 2
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Unit 3
Analytical Instruments based on separation Techniques
Total Teaching Hours – 10
Distribution of Theory Marks
R Level – 04
U Level – 08
A Level – 04
Total Marks – 16
Unit Outcomes (UOs) (in cognitive domain)
- Classify the chromatograph for the given techniques
- Describe the working principle of the given chromatograph.
- Identify the elements of the given chromatograph.
- Select the chromatograph for analyzing the given sample.
- Describe the working principle of the given mass spectrometer
- Select the mass spectrometer to analyze the given sample.
- Describe the procedure to troubleshoot the given separation technique based analytical instrument.
Topics and Sub-topics
- Principle of chromatography, Classification of chromatography,
- Gas Chromatography: Principle, diagram, Basic elements of GC, working, Application
- Liquid Chromatography : Principle, diagram , Basic elements of LC, working, Application
- Mass Spectrometer : diagram, working Principle, types: Magnetic deflection (Nier 60sector)type, Time of flight type, diagram, working, Applications –
- GCMS
- LCMS
Unit 4
Industrial gas Analyzer
Total Teaching Hours – 10
Distribution of Theory Marks
R Level – 04
U Level – 08
A Level – 04
Total Marks – 16
Unit Outcomes (UOs) (in cognitive domain)
- Identify an electrode for given sample,
- Describe the working principle of given gas analyzer.
- Select the gas analyzer for the given gas sample.
- Categorize the gas analyzer for given industrial application.
- Describe the procedure to troubleshoot the given Industrial gas Analyzer
Topics and Sub-topics
- Electrodes: Glass, Calomel, pO2, pCO2, construction and working, pH meter, Principle, construction & working.
- Complete Blood gas Analyzer for measurement of pH, pCO2,pO2, TCO2,HCO3,Base excess – Block diagram of complete blood gas analyzer, working.
- Infrared gas Analyzer: Principle, Block diagram working. applications.
- Thermal conductivity Analyzer: Principle, diagram, working, applications.
- Paramagnetic Oxygen Analyzer
Unit 5
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Suggested Student Activities:
Other than the classroom and laboratory learning, following are the suggested student-related co-curricular activities which can be undertaken to accelerate the attainment of the various outcomes in this course: Students should conduct following activities in group and prepare reports of about 5 pages for each activity, also collect/record physical evidences for their (student’s) portfolio which will be useful fortheir placement interviews:
- Visit to pathological laboratories to understand the operation of various analytical equipment.
- Visit to industrial laboratories to understand the working of various analytical equipments.
- Visit to PUC(Pollution under control) to measure the concentration of pollutants
- Do internet survey and use various meters to calibrate analytical equipment
- Read the safety precautions to operate various analytical equipment.
- Library/Internet survey of advanced analytical equipment.
- Prepare power point presentation or animation for understanding the concept of working of analytical instruments.
Suggested Special Instructional Strategies:
These are sample strategies, which the teacher can use to accelerate the attainment of the various outcomes in this course:
- Massive open online courses (MOOCs) may be used to teach various topics/sub topics.
- ‘L’ in item No. 4 does not mean only the traditional lecture method, but different types of teaching methods and media that are to be employed to develop the outcomes.
- About 15-20% of the topics/sub-topics which is relatively simpler or descriptive in nature is to be given to the students for self-directed learning and assess the development of the COs through classroom presentations (see implementation guideline for details).
- With respect to item No. 10, teachers need to ensure to create opportunities and provisions for co-curricular activities.
- Guide students in undertaking micro-projects.
- Use proper equivalent analogy to explain different concepts.
- Use Flash/Animations to explain working principle of analytical instrument.
Suggested Micro-Projects
For the complete Syllabus, results, class timetable, and many other features kindly download the iStudy App
It is a lightweight, easy to use, no images, and no pdfs platform to make students’s lives easier..
Suggested Learning Resources:
- Handbook of Analytical Instrumentation Khandpur R. S. McGraw Hill Education, New Delhi, 2009, ISBN -13:978-0-07-060460-5 ISBN-10:0-07-060460-6
- Analytical Instrumentation Liptak Bela G. CRC Press,1994,ISBN:9780801983979
- Instrumental methods of analysis Willard Merrit Dean CRC Press ISBN-9780534290153
- Instrumental method of chemical analysis Ewing E. W. McGraw Hill Education, New Delhi, ISBN-9780070198531
- Introduction to instrumental analysis Braun Robert D. McGraw Hill Education, New Delhi, ISBN-978007100472
- Principle of instrumental analysis Skoog;Holler&Nie man Sunder C ISBN-9781305577213
- Bioinstrumentation L. Veerakumari MJP Publishers,Chennai2006, ISBN 81-8094-018-7
Software/Learning Websites:
- http://vlab.amrita.edu/?sub=l&brch=194&sim:=802&cnt=4
- http: //vl ab. amri ta. edu/? sub= 1 &brch= 192
- http://ccnsb06-iiith.vlabs.ac.in/exp6 10/IR Powder_exp6.swf
- http://ccnsb06-iiith.vlabs.ac.in/exp7/index.php
- http://ccnsb06-iiith.vlabs.ac.in/exp8/index.php
- http://ccnsb06-iiith.vlabs.ac.in/exp9/index.php
- http://ccnsb06-iiith.vlabs.ac.in/exp5/index.php
- http://ccnsb06-iiith.vlabs.ac.in/expl0/index.php
- http://vlab.amrita.edu/?sub= 1 &brch= 195&sim=3 59&cnt= 1
- https://www.youtube.com/watch?v=bVKASwadjQY
For detail Syllabus of all other subjects of Instrumentation, 5th Sem, scheme I -, visit Instrumentation 5th Sem Syllabus for I – Scheme.
For all Instrumentation results, visit MSBTE Instrumentation all semester results.