Technology of Inorganic Chemicals detailed Syllabus for Chemical Engineering (CH), I – scheme has been taken from the MSBTE official website and presented for the diploma students. For Subject Code, Subject Name, Lectures, Tutorial, Practical/Drawing, Credits, Theory (Max & Min) Marks, Practical (Max & Min) Marks, Total Marks, and other information, do visit full semester subjects post given below.
For all other Diploma in Chemical Engineering (CH) Syllabus for 3rd Sem I – Scheme MSBTE, do visit Diploma in Chemical Engineering (CH) Syllabus for 3rd Sem I – Scheme MSBTE Subjects. The detailed Syllabus for technology of inorganic chemicals is as follows.
Rationale:
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Competency:
The aim of this course is to help the students to attain the following industry identified competency through various teaching learning experiences:
- Apply basic concepts of inorganic chemistry in chemical engineering applications.
Course Outcomes:
The theory and relevant soft skills associated with this course are to be taught and implemented, so that the student demonstrates the following industry oriented COs associated with the above mentioned competency:
- Manufacture the inorganic acids in chemical process industries.
- Prepare Ammonia-based fertilizers in chemical process industries.
- Select the raw material for Phosphate based fertilizer manufacturing.
- Prepare Caustic soda in chemical process industries.
- Synthesize the Cement of known composition.
- Manufacture industrially important gases.
Suggested Exercises:
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Instruments Required:
The major equipment with broad specification mentioned here will usher in uniformity in conduct of experiments, as well as aid to procure equipment by authorities concerned.
Equipment Name with Broad Specifications
- Beakers (100ml to 500ml.
- Burette with stand, 50 ml
- Thermometer
- Hydrometer
- Conical flask (100 to250ml..
- pipette (10 to 25ml.
- Measuring cylinder (10 to 50ml.
- Weighing balance
- Ceramic crucible
- Laboratory oven up to temperature range of 250 C
- Bottles (250ml.
- Test Tube (20ml.
Unit 1
Inorganic Acids
Total Teaching Hours – 12
Distribution of Theory Marks
R Level – 02
U Level – 04
A Level – 06
Total Marks – 12
Unit Outcomes (UOs) (in cognitive domain)
- Identify raw material for the manufacturing of the given acid with justification.
- Describe with sketches the process flow diagram for the manufacturing of the given acid.
- Identify the components of chemical reaction for the given acid manufacturing with justification.
- Describe with sketches the evaporation process for manufacturing the given acid.
Topics and Sub-topics
- Hydrochloric acid: Raw materials, Chemical reaction, manufacturing process, Process flow diagram, Industrial applications, Economics, Manufacturing industries.
- Sulfuric acid: Raw materials, Chemical reaction, manufacturing process. Process flow diagram, Industrial applications, Economics, Manufacturing industries.
- Nitric acid: Raw materials. Chemical reaction, manufacturing process, Process flow diagram Industrial applications, Economics, Manufacturing industries.
- Phosphoric Acid: Raw materials, Chemical reaction, manufacturing process. Process flow diagram. Industrial applications. Economics, Manufacturing industries.
Unit 2
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Unit 3
Phosphorous based fertilizer
Total Teaching Hours – 12
Distribution of Theory Marks
R Level – 02
U Level – 04
A Level – 06
Total Marks – 12
Unit Outcomes (UOs) (in cognitive domain)
- Identify the applications of the given phosphorous with justification.
- Eliminate the hydrofluoric acid from the given chemical manufacturing process.
- Describe with sketches the manufacturing of the given fertiliser.
- Describe the conversion process for the given MAPDAP.
Topics and Sub-topics
- Phosphorous: Raw materials, Chemical reaction, manufacturing process, Process flow diagram, Industrial applications, Economics and Manufacturing industries
- Super phosphate: Raw materials, Chemical reaction, Manufacturing process, Process flow diagram, Industrial applications, Economics and Manufacturing industries
- Triple Superphosphate: Raw materials. Chemical reaction, manufacturing process. Process flow diagram, Industrial applications. Economics and Manufacturing industries
- Di-Ammonium phosphate: Raw materials, chemical reaction, manufacturing process, process flow diagram, industrial applications, economics and manufacturing industries
Unit 4
Potassium based fertilizer and Chloro Alkali Material
Total Teaching Hours – 13
Distribution of Theory Marks
R Level – 02
U Level – 04
A Level – 06
Total Marks – 12
Unit Outcomes (UOs) (in cognitive domain.
- Identify the components of mixed fertilizers for the given grades.
- Apply the relevant chemical reaction for the given Potassium fertilizer.
- Apply electrolysis of brine for the given application.
- Identify raw material for manufacturing of Caustic Soda of the.given strength.
Topics and Sub-topics
- Mixed fertilizer: Definition, grades, Application
- Potassium fertilizer: Raw materials, Chemical reaction, Process flow diagram, Manufacturing Process, Industrial applications. Economics and manufacturing industries.
- Chlorine and caustic soda: Raw materials, Chemical reaction, Process flow diagram, Manufacturing Process, Industrial applications, Economics and Manufacturing industries
- Soda Ash: Raw materials, Chemical reaction. Process flow diagram, Manufacturing Process, Industrial applications. Economics and Manufacturing industries
Unit 5
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Unit 6
Industrial Gases
Total Teaching Hours – 08
Distribution of Theory Marks
R Level – 02
U Level – 04
A Level – 06
Total Marks – 12
Unit Outcomes (UOs) (in cognitive domain)
- Describe the principle of liquefaction of air for the given composition.
- Explain the heat economy for the given waste heat boiler.
- Describe the concept of absorption for the given manufacturing process.
- Apply the process of hydrolysis for the given system.
Topics and Sub-topics
- Oxygen and Nitrogen: Principle, Lindes and Claudes method
- Hydrogen: Preparation from water gas.
- Carbon dioxide: from flue gases.
- Acetylene: from calcium carbide
- Water gas: preparation using coal
- Producer Gas: By using coal.
Note: To attain the COs and competency, above listed Unit Outcomes (UOs) need to he undertaken to achieve the ‘Application Level of Blooms ‘Cognitive Domain Taxonomy
Note:
Legends: R= Remember, U=lJnderstand, A =Apply and above (Blooms Revised taxonomy)
Note: This specification table provides general guidelines to assist student for their learning and to teachers to teach and assess students with respect to attainment of UOs. The actual distribution of marks at different’ taxonomy levels (of R, U and A) in the question paper may vary from above table.
Suggested Student Activities:
Other than the classroom and laboratory learning, following are the suggested student-related co-curricular activities which can be undertaken to accelerate the attainment of the various outcomes in this course: Students should conduct following activities in group and prepare reports of about 5 pages for each activity, also collect/record physical evidences for their (students) portfolio which will be useful for their placement interviews:
- Identify engineering problems based on real world problems and solve with the use of free tutorial available on the internet.
- Use softwares and digital resources for related topics.
Suggested Special Instructional Strategies:
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Suggested Micro-Projects
Only one micro-project is planned to be undertaken by a student that needs to be assigned to him/her in the beginning of the semester. In the first four semesters, the micro-project are group-based. However, in the fifth and sixth semesters, it should be preferably be individually undertaken to build up the skill and confidence in every student to become problem solver so that s/he contributes to the projects of the industry. In special situations where groups have to be formed for micro-projects, the number of students in the group should not exceed three.
The micro-project could be industry application based, internet-based, workshopbased, laboratory-based or field-based. Each micro-project should encompass two or more COs which are in fact, an integration of PrOs, UOs and ADOs. Each student will have to maintain dated work diary consisting of individual contribution in the project work and give a seminar presentation of it before submission. The total duration of the micro-project should not be less than 16 (sixteen) student engagement hours during the course. The student ought to submit micro-project by the end of the semester to develop the industry oriented COs.
A suggestive list of micro-projects are given here. Similar micro-projects could be added by the concerned faculty:
- Visit to fertilizer plant : Visit nearby fertilizer plant and prepare block diagram of process, List of unit operations used, Schematic sketches of each stage of manufacturing processes and process description.
- Internet based assignment: Prepare a power point presentation on a topic List of inorganic chemicals manufacturing industries in India
- Chemical Engineering aspects in cement Industry ( Internet based assignment):Identify a cement Industry, Make the list of product manufactured, make the list of unit operations and unit processes, Describe the identified unit operations and unit processes, Identify the job role for a chemical engineer in Cement industry, Safety precautions.
- Collection of different fertilizer sample from market. (Field assignment ) :Collect two samples from four companies. Classify the samples on the basis of content, identify the location of industry, Prepare a report based on content and cost
- Testing procedure of PUC: Observe procedure of testing for four wheelers, Study pollutants present, Prepare a report for five vehicles.
- Profile of PSUs: Prepare a chart demonstrating profile of typical public sector organization, RCF, IFFCO, ZUARI, containing product manufactured, block diagram, technical specification of product manufactured, safety aspects related to product, unit operations and processes involved.
Suggested Learning Resources:
- Drydens outline of Chemical Technology. Gopal Rao, M. and Sitting, Marshal East West Publisher, London, 2010, ISBN: 9788185938790,
- Shreves Chemical Process Industries. Austin, George T. McGraw-Hill Book Company, Tacoma, WA, U.S.A, 1984 ISBN: 9780070571471
- Unit Process of Organic synthesis. Groggins, P.H. Me Graw Hill International, New York, 1958 ISBN: 8185938792
- Reactions and Synthesis Francis A. Carey, Ri chard J. Sundberg Springer, Basel, 2012, ISBN: 1-4613-9798-7
Software/Learning Websites:
For the complete Syllabus, results, class timetable, and many other features kindly download the iStudy App
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For detail Syllabus of all other subjects of Chemical Engineering, I – scheme do visit Chemical Engineering 3rd Sem Syllabus for I – scheme.
For all Chemical Engineering results, visit MSBTE Chemical Engineering all semester results direct links.