For detailed syllabus of all other subjects of Chemical Engineering 6th Sem, 2015 curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

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Wishing you great luck ahead.

For Chemical Engineering 6th Sem scheme and its subjects, do visit CH 6th Sem 2015 revision scheme. The detailed syllabus of project & seminar ii is as follows.

Course Objectives:

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Selection of Project:

1. Select programme related project which has relevance to today’s industry, preferably with a social relevance.
2. Suggested type of Projects :
   1. Providing technical service to industry
   2. Entrepreneurship development
3. Project should be feasible at Diploma level and economically viable
4. Only projects which can be developed by the Diploma students need be selected. Support of external agencies not permitted

Guidelines for Project Work:

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Format for the preparation of Project work :

1. Cover Page as per format
2. Acknowledgement
3. Certificate of the Project Guide
4. Synopsys of the Project
5. Main Report
   1. Objective & Scope of the Project
   2. Theoretical Background
   3. Definition of Problem
   4. Methodology adopted, System Implementation & Details -Hardware/Software/Machinery/Equipment/used

For detailed syllabus of all other subjects of Chemical Engineering, 2015 revision curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

To see the syllabus of all other branches of diploma 2015 revision curriculum do visit all branches of SITTTR diploma 2015 revision.

For Chemical Engineering 6th Sem scheme and its subjects, do visit CH 6th Sem 2015 revision scheme. The detailed syllabus of mass transfer lab is as follows.

Course Outcomes:

1. Determine mass transfer coefficients.
2. Set up distillation column. Verify various theorem related to distillation
3. Demonstrate various leaching operations.
4. Identify extraction methods for oil seeds. Select suitable solvent for extraction.
5. Determine humidity.

SPECIFIC OUTCOMES:

LIST OF EXPERIMENTS

1. Verify Rayleigh’s equation .
2. Determine vaporization efficiency of Steam Distillation.
3. Determine stage efficiency of Single Stage Leaching.
4. Determine overall efficiency of Multi Stage Leaching.
5. Determine the percentage of oil extracted Oil seed.
6. Determine Ternary Liquid Equilibrium.
7. Determine Drying rate curve using Atmospheric batch Dryer.
8. Determination of Humidity Psychometric method.

DEMONSTRATION EXPERIMENTS

1. Understand Fractional Distillation Column.
2. Know the Extraction Battery.

For detailed syllabus of all other subjects of Chemical Engineering, 2015 revision curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

To see the syllabus of all other branches of diploma 2015 revision curriculum do visit all branches of SITTTR diploma 2015 revision.

For Chemical Engineering 6th Sem scheme and its subjects, do visit CH 6th Sem 2015 revision scheme. The detailed syllabus of particle technology lab is as follows.

Course Outcomes:

1. Determine particle size distribution of particulate solid by different methods
2. Estimate the area of continuous thickner by conducting batch sedimentation test
3. Demonstrate the working of equipments used for various mechanical operations

SPECIFIC OUTCOMES

1. Determine particle size distribution of particulate solid by various methods
   1. Determine particle size distribution of particulate solid using sieve analysis
   2. Determine the effectiveness of screen using sieve analysis
   3. Determine particle size distribution of particulate solid using pipette analysis
   4. Determine particle size distribution of particulate solid using beaker decantation
2. Estimate the area of continuous thickner by conducting batch sedimentation test
3. Demonstrate the working of equipments used for various mechanical operations
   1. Ball mill
   2. Jaw Crusher
   3. Plate and Frame Filter Press
   4. Froth Floatation Cell
   5. Super Centrifuge

For detailed syllabus of all other subjects of Chemical Engineering, 2015 revision curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

To see the syllabus of all other branches of diploma 2015 revision curriculum do visit all branches of SITTTR diploma 2015 revision.

For Chemical Engineering 6th Sem scheme and its subjects, do visit CH 6th Sem 2015 revision scheme. The detailed syllabus of rubber technology is as follows.

Course Outcomes:

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SPECIFIC OUTCOMES

MODULE- I

1. Understand the importance, collecting and processing of NR latex
   1. State the importance of NR as a raw material
   2. List out the major sources of NR
   3. Define tapping
   4. List the factors affecting tapping efficiency
   5. Explain the uniqueness of NR
   6. Explain Discuss the possibilities of blending NR with other rubbers
   7. State the applications of NR
2. Understand the preservation and concentration of NR latex
   1. Define latex
   2. Explain the colloidal nature of latex
   3. Describe the composition of NR latex
   4. State the necessity for preservation of latex
   5. State the requisites of an ideal preservative
   6. Define the terms preservative, short term preservatives and long term preservatives
   7. Explain Discuss the coagulation and method of coagulation of latex
   8. Explain pre-coagulation and use of various anticoagulants
   9. Describe De level Centrifuge with a diagram
   10. State the need for concentration of latex
   11. List the various concentration methods
   12. Explain the principle of creaming of latex
   13. Explain the various creaming agents used (Tamarind seed powder, Sodium alginate, Ammonium alginate etc) – Definition, examples, their actions, possible mechanisms, their preparation, dosage and method of incorporation
   14. Explain the process of centrifuging of latex with flow chart
   15. Give the meaning of efficiency of centrifuging
   16. State the factors affecting centrifuging
   17. Explain skim latex and skim rubber
   18. Mention the uses of skim rubber
3. Study the processing of NR latex into dry marketable forms
   1. Define Ribbed smoked sheets (R.S.S)
   2. Explain the relevance of grading of sheet rubber
   3. Define crepe rubber
   4. Define tyre rubber
   5. Explain the preparation, properties and advantages of tyre rubber

MODULE – II

1. Understand general characteristics of elastomers
   1. Narrate brief history of NR& SR
   2. Classify SR with reference to their applications.
   3. Explain rubber elasticity
   4. Explain general characteristics of SR
   5. Compare elastomers with other polymers like plastics and fibers.
   6. Define elastomers with reference to extensibility and recovery, Glass Transition temperature (Tg) etc.
2. Understand the structure, preparation and properties of monomers & production Properties and applications of various general-purpose synthetic rubbers.
   1. Explain the structure, production and properties of the following monomers styrene, butadiene, isoprene, isobutylene, ethylene and propylene.
   2. Explain the structure, production, properties (raw and vulcanisate), curing systems, compounding, processing, grades, trade names and application general purpose synthetic rubbers like
   3. Styrene butadiene rubbers (SBR). Poly butadiene rubber (BR), Isoprene rubber(IR)Butyl (IIR ) EPDM
   4. Explain the structure, production, properties (Raw and Vulcanisate), Cure Systems, pounding, processing, grades, trade names and applications of special purpose rubbers
   5. NBR and Discuss the effect of Acrylonitrile, butadiene ratio on the properties of NBR
   6. CR
      1. CSM
      2. Polysulphide rubber
      3. Silicone rubber
      4. Polyurethane rubber

MODULE-III

1. Understand principles of compounding
   1. Define compounding and its objective
   2. Prepare a general recipe for product manufacturing
   3. List out the compounding ingredients
   4. Explain base polymer and its function in a compound
   5. Explain vulcanizing agent and its function
   6. State the role of curing system in Recipe
   7. Describe the function of accelerators and their classification
   8. Explain activators and their function and application
   9. Analyze the role of other ingredient such as filler, plasticiser, softener and other special additives used in rubber industry
2. Comprehend the theory of vulcanization
   1. Explain the changes that occur in a Rubber compound due to vulcanization
   2. Explain sulphur vulcanization
   3. Describe the different types of cross-links and their effect on vulcanisate properties
   4. Explain the theory of vulcanization
   5. Distinguish low sulphur vulcanization and non-sulphur vulcanization with example
   6. Distinguish CV, EV and SEV
   7. Describe the curing system used for NR and SR
   8. Discuss sulphur system and non sulphur system for olefin and non olefin rubbers
3. Understand preparation, properties & application of compounding ingredients
   1. Explain the classification of fillers.
   2. Describe the preparation and application of various non black fillers like inorganic fillers fibrous filler, organic fillers and resinous filler
   3. Classify carbon black
   4. Describe the methods of manufacturing various types of carbon black
   5. State ASTM D 1765 for grading of carbon black
   6. Summarize the properties of carbon black particle size, structure, chemical and physical nature porosity etc
   7. Describe the procedures for determination of particle size and structure of carbon black
   8. Define degradation
   9. Describe the importance of antidegradants
   10. List the factors affecting degradation
   11. Explain staining and non staining Antioxidants & antiozonants
   12. Explain how plasticizers are classified. Give examples
   13. Explain the effect of plasticizer on Vulcanisate properties
   14. List out the special purpose compounding ingredients used in Rubber compounding.
4. Understand different vulcanization method other than molding
   1. Explain radiation vulcanization
   2. Explain different methods of batch vulcanization methods
   3. Give examples of product manufactured by batch vulcanization method
   4. Explain continuous vulcanization methods
   5. Explain Roto cure with an example
   6. Explain fluidized bed, microwave curing and give examples of each method
   7. Explain steam tube vulcanization

MODULE-IV

1. RUBBER PRODUCTS
   1. Name the major rubber products manufacturing industries in India
   2. Compare the per capita consumption of rubber in India and that of other countries
   3. Summarise the statistics relating to the production, consumption and export of dry rubber products.
   4. Classify rubber products according to their application
   5. Mention the different steps involved in the production of dry rubber products
2. Molded Products
   1. Name important compression molded products
   2. Explain the design, compounding and production details of automobile bushes, mats, paperweights, IB Caps, Door bushes, Nipples, hot water bags
   3. Discuss the design criteria and design of compounds for above products
   4. List hard-rubber products
   5. Explain the chemistry and technology of hard rubber (ebonite) production.
   6. Explain compounding and production of battery box containers
3. Expanded Products
   1. Define cellular rubber
   2. Classify different cellular rubber
   3. State the principle of creating cellular structure in rubber
   4. Distinguish closed and open cell cellular products
4. Extruded Products
   1. List the various extruded products
   2. Describe the manufacture of automobile channels
   3. Explain the manufacture of rubber tubing
   4. Discuss the compound design for the above products
   5. Identify major defects and remedies in the manufacturing of the above products
5. Calendared products
   1. List out various calendared products
   2. Distinguish between supported and unsupported sheets
   3. Describe the manufacture of hospital sheeting and supported sheeting
   4. Explain profile calendaring with examples
   5. Describe the design criteria for various calendared products
   6. Identify the major defects in calendared sheets

MODULE-I

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MODULE II

Monomers – Preparation and properties of the monomers-styrene, butadiene, isoprene, Isobutylene, ethylene, propylene-structure of Diene monomers-Detailed study of SBR,PBD ,IR,EPDM,& IIR-Monomers – Preparation and properties of the monomers-Acrylonitrile , chloroprene ,-SBR, NBR, Butadiene hydroxy terminated SBR, NBR, Butadiene. -Thermo Plastic Eleastomers-Thermo plastic elastomers, definition, Advantages,modification of elastomers to thermoplastic elastomers. Study of thermoplastic SBR, Ethylene Vinyl acetate, Thermo polyurethane.Blends-Definitions – Advantages, Procedure, Blending for specific properties, study of NR – PBD, NR-SBR-PBD, NR-EVA, NBR-PVC, NR-HSR

MODULE-III

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MODULE IV

Molded Products-Introduction to rubber products:Production methods, compound design -Automobile Expanded Products: Types of blowing agents and their comparison- Compounding and Molding of Cellular rubber products, MC, Hawaii sponge -Typical formulations- Extruded Products: Automobile treads, channels, inner tubes, LPG tubes etc- Compound design, Typical formulations, Methods of manufacture. Calendered Products: Supported and unsupported sheeting, Hospital sheeting, Profile calendered products- Design criteria, compound design, typical formulations. Rubber to Metal bonded products-Principle of bonding rubber to metal and textile fibers. Production of rubber covered rolls-metal preparation- compound preparation, assembling curing, finishing-Tank lining- Production method, compounding, compound design. Production of typewriter rolls, Rice polisher, Textile roller.

Reference Books:

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For detailed syllabus of all other subjects of Chemical Engineering, 2015 revision curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

To see the syllabus of all other branches of diploma 2015 revision curriculum do visit all branches of SITTTR diploma 2015 revision.

For Chemical Engineering 6th Sem scheme and its subjects, do visit CH 6th Sem 2015 revision scheme. The detailed syllabus of plan utilities and maintenance is as follows.

Course Outcomes:

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SPECIFIC OUTCOME

MODULE-I UTILITY AIR, WATER, AND STEAM

1. Understand utility Air and water
   1. Name the air handling Equipments
   2. Preparation methods of Instrument air
   3. Discuss about heating and cooling of air
2. Comprehend Importance of water in chemical industries and water purification process
   1. List the source of water
   2. List the characteristics of water
   3. Define hardness
   4. Define temporary and permanent hardness
   5. State the disadvantages of hard water
   6. State the scale and sludge formation in boilers
   7. List the disadvantages of scale formation
   8. Define caustic embrittelment
   9. Explain the following softening methods
      1. lime soda process
      2. zeolite process.
   10. List advantages disadvantages cold and hot lime soda process
   11. Explain the ion exchange process
   12. Explain the method of municipal water treatment.
   13. Describe the Production of cooling Water and chilled water
   14. Explain the methods of distribution of cooling water
   15. Describe preparation of Boiler Feed Water.

MODULE- II Steam & Steam Generators

1. Understand the various properties of steam
   1. Explain the formation of steam under constant pressure.
   2. State the effect of pressure on temperature.
   3. Distinguish the wet steam, dry steam and super heated steam.
   4. Explain the properties of steam such as sensible heat, latent heat, total heat ofsteam, superheat and dryness fractions.
2. Understand the working of steam Generators
   1. Define a boiler.
   2. Explain the functions of a boiler.
   3. Distinguish between fire tube boiler and water tube boiler.
   4. Distinguish between low pressure boiler and high pressure boiler.
   5. Describe with line diagram the construction and working of a Simple Vertical Boiler and Cochran boiler, Babcock and Wilcox boiler, la -Mont Boiler and Benson boiler.
   6. Compare the smoke tube and water tube Boiler.
   7. List the specification of a boiler.
   8. State the function of boiler mountings such as stop valve, safety valve, water level indicator, pressure gauge and fusible plug etc. with line sketches.
   9. Explain the functions of boiler accessories such as economizer, feed pump, super heater and air pre-heater etc. with simple sketch
   10. Explain the developments such as draft, natural draft, induced draft, forced draft and balanced draft.

MODULE – III Operational Maintenance of Chemical Plant equipments

1. Understand the principles of maintenance management
   1. List the need for maintenance.
   2. List the three types of maintenance.
   3. Prepare a sample maintenance schedule for any equipment.
   4. Describe the cost factors in maintenance.
   5. List the main elements in a maintenance records.
   6. List the tree types of equipment replacement.
2. Comprehend maintenance of Chemical Plant equipments
   1. List the methods of cleaning tubular equipments.
   2. State why cleaning of tubular equipment is essential.
   3. Explain method and procedures of chemical cleaning of tubular equipment.
   4. Describe the mechanical methods of cleaning tubular equipments.
   5. List the method for cleaning towers and columns.
   6. Explain the common causes of troubles and remedial action in the following equipments: Centrifugal pumps, Reciprocating compressor, Filter press, Agitator
   7. Explain the decoking methods of furnace tubes.
3. Know start up and commissioning of some plant equipments
   1. Describe the procedure for starting of centrifugal pumps.
   2. List the precautions to be taken before starting the reciprocating pump.
   3. List the precautions to be taken before starting of the reciprocating compressor.
   4. Explain various steps to be taken for the start up and commissioning of the heater.
   5. Explain various steps to be taken for start up and commissioning of a distillation column.
   6. Select various steps to be taken for start up and commissioning of the Absorption columns.
4. Understand chemical plant inspection
   1. Explain the precautions to be taken before opening and entry in the vessels for cleaning.
   2. List the types of inspections.
   3. Explain conventional monitoring methods.
   4. List the standard testing methods of a high pressure vessels before and after fabrication.
   5. List the non-destructive testing methods.
   6. Describe the ultrasonic test for pressure vessel.
   7. Describe the radiographic test for pressure vessel.

MODULE – IV Plant Location and Layout.

1. Know the basic principles in location and layout of a chemical plant.
   1. List the points to be considered in the location of a big chemical plant.
   2. Identify the role of raw materials, transportation and power supply in the location of a Chemical plant.
   3. Explain the community factors in the location of a chemical plant.
   4. State the waste disposal and water supply in the location of a chemical plant.
   5. Explain the factors to be considered in the preparations of a plant lay out.
   6. Draw a plant lay out for a chemical plant.
   7. List the safety factors involved in plant layout.
   8. Locate a canteen, ETP, Boiler house, in a typical layout and justify the location.
   9. List the methods of preparing a plant layout and explain any one method.
   10. Explain master plot plan and unit plot plan.
   11. Draw a typical master plot plan of a plant you know.
   12. Explain the guide lines for preparing a master plot plan and unit plot plan
   13. Illustrate the scale model method of preparing plot plans.
   14. Draw sketches of different types of chemical plant buildings.
   15. Differentiate between housed and Un housed plants.
   16. Explain the advantages of multi storied construction over single storied construction.
   17. Explain chemical plant roofs and floorings.
   18. Describe the methods of providing artificial and natural ventilation and lighting.

MODULE I UTILITY- AIR AND WATER

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MODULE II PROPERTIES OF STEAM & BOILERS

Properties of steam – Explanation of properties of steam such as total heat of water – latent heattotal heat of steam- super heat – dryness fraction. Function of boilers – classification – working principle – fire tube and water tube boilers – Simple vertical boiler – Cochran boiler- Babcock and Wilcox boiler High pressure boilers – Benson boiler – Lamont boiler – Boiler mountings -accessories.

MODULE III OPERATIONAL MAINTENANCE OF CHEMICAL PLANT EQUIPMENTS

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MODULE IV PLANT LOCATION AND LAY-OUT

Location of Chemical Plant – Important Factors considering Plant Location and Plant Lay-out – Master Plot Plan and Unit Plot Plan – Chemical Plant -Buildings – Roofing – Flooring -Ventilation and Illuminations.

Reference Books:

For the complete syllabus, results, class timetable, and many other features kindly download the iStudy App
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For detailed syllabus of all other subjects of Chemical Engineering, 2015 revision curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

To see the syllabus of all other branches of diploma 2015 revision curriculum do visit all branches of SITTTR diploma 2015 revision.

For Chemical Engineering 6th Sem scheme and its subjects, do visit CH 6th Sem 2015 revision scheme. The detailed syllabus of bio-chemical engineering is as follows.

Course Outcomes:

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SPECIFIC OUTCOMES

MODULE – I BIO-PROCESS FUNDAMENTALS

1. Know the bio-process fundamentals
   1. Define Biochemical Engineering.
   2. Define micro biology.
   3. List the applications of bio- technology
   4. Describe integrated bio-process
   5. Classify the organism
   6. Draw the figure of simplified classification of ancestors.
   7. Define bio-molecules
   8. Explain in detail, the structure of Prokaryotic and Eukaryotic cells with figure.
   9. Identify the micro organisms -Bacteria, Viruses, Fungi, Algae, and Protozoa.
   10. Describe the classification, function and properties of Lipids.
   11. Explain the function and properties of Fatty acids.
   12. Describe the function and properties of steroids.
   13. Explain separation and purification of Proteins.
   14. Describe the properties and function of Vitamins.
   15. Explain the properties and function of Carbohydrates.
   16. Describe the function and properties of DNA and RNA.

MODULE – II ENZYMES

1. Understand the functions of Enzymes.
   1. Define enzyme.
   2. Explain the function of Enzymes as biological catalyst.
   3. List the terms associated with enzymology
   4. Describe the chemical theories behind the functioning of enzymes
   5. Define enzyme specificity.
   6. Explain different types of Enzyme specificity.
   7. Define active site of the enzyme.
   8. Explain Fischer Lock and Key hypothesis in Enzymes.
   9. Explain immobilization of Enzymes.
   10. Name the important Enzyme immobilization methods.
   11. Describe different methods of immobilization of Enzymes.
   12. Explain the properties of immobilized Enzymes.
   13. Explain the types of reactors used for Enzyme immobilization with a neat fig
   14. Classify various type of ideal flow reactors
   15. Classify the bio-reactors based on feeding mechanism.
   16. Explain the various industrial application of enzymes

MODULE – III FERMENTATION

1. Understand various fermentation processes
   1. Define fermentation.
   2. State the requirements of fermentation process.
   3. Draw a schematic representation of fermation process.
   4. Explain the constructional details of a fermenter with a neat sketch
   5. Explain the controlling and monitoring parameters of fermenter.
   6. Describe anaerobic and aerobic fermentation process.
   7. Distinguish between anaerobic and aerobic fermentation process.
   8. Describe solid state fermentation.
   9. State the advantages of solid state fermentation.
   10. Explain submerged fermentation .
   11. List the advantages of sub merged fermentation
   12. Differentiate between solid state fermentation and submerged fermentation.
   13. List the applications of solid state and submerged fermentation.
   14. State various types bioreactors
   15. Explain fluidized bed reactors and air lift reactors
   16. Describe the manufacture of ethyl alcohol by fermentation of molasses
   17. Explain the production of antibiotics through fermentation.
   18. Describe the manufacture of penicillin.

MODULE – IV RECOVERY & PURIFICATION OF PRODUCTS

1. Understand the importance of downstream process steps in bio processing
   1. List the various unit operations come across downstream processing
   2. Define membrane
   3. List the different types of membrane separation process
   4. State the advantages and disadvantages of membrane separation process
   5. List the polymeric materials that can be used as membranes
   6. State the important types of membranes
   7. State the characteristics of good membrane
   8. Explain the different types of membrane module
   9. List different types of Chromatographic process
   10. Describe in detail the affinity chromatographic process
   11. Explain the various application of Chromatographic separation process
   12. Explain the Dialysis process and mention its applications.
   13. Describe Microfiltration and its application
   14. Explain Nanofiltration and its application
   15. Explain ultra filtration and mention its application
   16. Describe reverse osmosis process and mention its applications

MODULE I

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MODULE II

Enzymes-nomenclature and classification- Biological catalyst- Enzymes specificity-Active site-Enzyme immobilization. Different types reactors-ideal flow-feeding mechanism- properties and applications of immobilized enzymes.

MODULE III

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MODULE IV

Downstream processes-membrane-types of membranes-separation processes- dialysischromatography-micro filtration-nano filtration- ultra filtration- reverse osmosis.

Reference Books:

For the complete syllabus, results, class timetable, and many other features kindly download the iStudy App
It is a lightweight, easy to use, no images, and no pdfs platform to make students’s lives easier.
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For detailed syllabus of all other subjects of Chemical Engineering, 2015 revision curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

To see the syllabus of all other branches of diploma 2015 revision curriculum do visit all branches of SITTTR diploma 2015 revision.

For Chemical Engineering 6th Sem scheme and its subjects, do visit CH 6th Sem 2015 revision scheme. The detailed syllabus of instrumentation & process control is as follows.

Course Outcomes:

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SPECIFIC OUTCOMES

MODULE – I Measuring instrument for Temperature, Pressure, Flow and Level measurement

1. Understand the importance of instrumentation in chemical process industries
   1. List important process variables in chemical industry
   2. Static and dynamic characteristics of instruments
   3. List the basic elements of measuring instrument
   4. Draw a sketch of measuring instrument and indicate the basic elements and explain the functions of these elements
   5. List the temperature measuring instruments
   6. Explain the working of pressure spring thermometers
   7. Explain the working of pneumatic balance pressure thermometer
   8. Explain the working of vapour pressure thermometers
   9. Explain the working principles of thermocouples – SEEBACK, THOMSON AND PETLIER effect
   10. List the commonly used thermocouple wires with their temperature range of measurement
   11. List the advantages and disadvantages of thermocouples
   12. Explain the principle and working of radiation pyrometers
   13. Explain the principle and working of optical pyrometers
2. Understand the working of pressure measuring instruments
   1. Explain the working principle of a ‘c’ type Bourden tube
   2. Explain the following gauges with sketch
      1. Me-leod gauge
      2. Pirani gauge
   3. Explain the working of Bellows gauge and diaphragm gauge
3. Understand the working of various flow measuring instruments
   1. Principles involved in various flow meters
   2. Explain the working of gas flow meter
4. Understand the working of various liquid level measuring instruments
   1. Explain the working of
      1. float type
      2. Diaphragm box
      3. Bubbler system
      4. Electronic signalling type
      5. Magnetic type

MODULE – II Measuring Instruments for specific gravity, Viscosity Humidity

1. Understand the working of instruments used for measuring viscosity, specific gravity ,humidity.
   1. Describe with sketches of the following viscosity measuring instruments
      1. Ostwald viscometer
      2. Continuous viscometer
   2. Describe with the sketch displacement meter for specific gravity measurement
   3. Describe with sketch hydrometer type density measuring Instrument
   4. List the various humidity measuring instruments
   5. Define – Absolute humidity, specific humidity, relative humidity, wet bulb and dry bulb Temperature, dew point temperature
   6. Explain with sketches of the following instruments
      1. Wet and dry bulb thermometer
      2. Hair hygrometer
      3. Electric hygrometer
      4. Dew point recorder
2. Understand the significance of pH in process industries
   1. List the pH scale, with pH of some known liquids
   2. Describe with sketches of glass electrode and calomelelectrode
   3. Explain the basic working principles of a pH meter
   4. List various types of sensing devices of pH meter
   5. Explain immersed type sensor for pH meter

MODULE-III Composition analysis methods

1. Understand the methods of composition analysis
   1. Define spectroscopy
   2. Classification of spectroscopy
   3. Describe with a sketch of an infrared spectrophotometer
   4. Application of infrared spectrophotometer
   5. Describe with a sketch an ultraviolet spectrophotometer
   6. Application of ultraviolet spectroscopy
   7. Describe with a sketch of a flame photometer and lists its application
   8. Advantages and drawbacks of flame photometer
   9. Describe with a sketch of a Mass spectrometer and lists its application
   10. Disadvantages of mass spectroscopy
   11. Describe with a sketch of Atomic Absorption spectroscopy and list its application
2. Understand chromatography and its classification
   1. Define chromatography
   2. List the advantages of chromatography
   3. Explain with sketch of adsorption chromatography
   4. Explain with sketch of Liquid column Chromatography
   5. Explain Gas Solid Chromatography and Gas Liquid Chromatography with neat sketch
   6. Comparison of GSC and GLC
   7. Explain with sketch of HPLC

MODULE – IV Automatic process control

1. Understand the important Process control variables and terms
   1. Define
      1. Controlled variable
      2. Manipulated variable
      3. Load variable
      4. Dead time
      5. transportation lag
      6. Resistance
      7. Capacitance
   2. Explain the following types of control action
      1. Proportional
      2. Integral
      3. Proportional integral
      4. Proportional Derivative
      5. PID
   3. Explain two position control and its working
   4. List various controlling methods
   5. Explain Closed loop system or feedback control system with neat fig and example.
   6. Explain Open loop system or feed forward control system with neat fig and example
   7. Differentiate different types of control actions and how they are selected with neat figure.
   8. Describe in detail the temperature control of an air oven with two position control
   9. Draw the Instrumentation diagram of the following
      1. extraction column
      2. Single effect evaporator
      3. chemical reactor
2. Understand Controllers and control valves
   1. Explain the important features of controllers
   2. Explain working of pressure regulator
   3. Explain the working of flapper nozzle pneumatic controllers
   4. Differentiate electronic and pneumatic controller
   5. Explain the working of various types control valve plugs
   6. Define final control element.
   7. List various forces acting on the output member of final control element.
   8. Explain fluid flow control valve with neat sketch
   9. Explain solenoid valve
3. Understand the computerized control system
   1. Explain a micro-processer with neat sketch
   2. Define analog and digital signal transmission
   3. State the functions of A/D converter and D/A converter
   4. Explain DCS with a neat diagram
   5. Explain the DCS components
   6. State the Application of DCS
   7. List advantages and limitations of DCS
   8. Explain the following
      1. Control components of SCADA
      2. Working of SCADA
      3. Comparison of SCADA with DCS
   9. Describe the requirements of digital control and information monitoring system
   10. Draw the standard symbols of instruments and controllers
   11. List the functions of control room instruments

MODULE – I

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MODULE – II

Understand the measuring instrument for viscosity, specific gravity, humidity Viscosity—Ostwald-continuous viscometer Sp. Gravity- Displacement meter, hydrometer Humidity Absolute humidity, specific humidity, relative humidity, wet bulb and dry bulb temperature, dewpoint temperature Dew point method, wet bulb method, hygrometry, electrical type. pH- significance- scale-liquids, Electrodes- glass, calomel, pH meter- principle-sensing elements-immersed type

MODULE – III

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MODULE – IV Process Control

Process -control variables-terms types of control action-proportional integral, PI-PD-PID process control system open and closed loop systems – block diagrams of back ward feed, forward feed controls – types of control modes – on-off, proportional, integral, derivative, and their combinations. Comparison of different types of controls- temperature control of air oven instrumentation diagrams- various controlling methods– feedback control- feed forward control- -, controllers-working of flapper nozzle Pneumatic control-Various control valve plugs-. Final control elements – control valves, actuators, fluid flow control valve Computerized Control and Instrumentation Diagrams Microprocessor Descriptive treatment of the following: – Analog and digital signal transmission, A/D, D/A converter, analog and digital computer control system – microprocessor, distributed control system -SCADA,Comparison of SCADA with DCS.

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For detailed syllabus of all other subjects of Chemical Engineering, 2015 revision curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

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For Chemical Engineering 6th Sem scheme and its subjects, do visit CH 6th Sem 2015 revision scheme. The detailed syllabus of particle technology is as follows.

Course Outcomes:

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SPECIFIC OUTCOMES

MODULE- I Filtration and Centrifugation

1. Understand filtration as a solid liquid separation
   1. Define filtration
   2. List the type of filters
   3. Discuss the working of sand filter
   4. Draw the sketch of plates and frames of filter press
   5. Draw the sketch of plate and frames in the filtering operation
   6. Discuss the working of plate and frame filter press
   7. Explain the washing of plate and frame filter press
   8. Explain the working of leaf filter
   9. Explain the working of Moore filter
   10. Explain the working of Rotary Drum Filter & Draw the sketch
2. Recognize the selection criteria of filters
   1. List the factors on which rate of filtration depends
   2. List the types of filter aids
   3. State the function of filter aids in filtration
   4. State the application of filter aids
   5. List the types of filter cakes
   6. Explain compressible and non-compressible filter cakes
   7. Explain constant pressure filtration
   8. Explain constant volume filtration
   9. St a t e the rate equation for constant pressure filtration
   10. Sta te term resistance of filter cake
   11. Compute the time of filtration using the rate equation
3. Understand the process Centrifugation
   1. List the classification of centrifuges
   2. Draw the sketch of top driven taken centrifuge
   3. Describe the working top driven batch centrifuge
   4. Describe the working of bottom driven centrifuge
   5. Draw the sketch of super centrifuge
   6. Describe the working of super centrifuge
   7. Draw the sketch of Disc centrifuge
   8. Describe the working of disc centrifuge

MODULE – II Size Reduction

1. Know the size reduction techniques
   1. Generalize the important of size reduction
   2. List the nature of materials to be crushed
   3. Discuss closed circuit grinding
   4. Discuss open circuit grinding
   5. List the classification of crushing and grinding equipments
2. Understand the working of crushing equipments
   1. Draw the sketch of Blake Jaw crusher
   2. Explain the working of Blake Jaw crusher
   3. Compare Blake and Dodge Jaw crusher
   4. Draw the sketch of gyratory crusher
   5. Explain the working of gyratory crusher
   6. Explain crushing rolls
   7. Draw the sketch of a smooth roll crusher
   8. Define the angle of Nip of crushing rolls
   9. Explain the theory behind the action of crushing rolls
   10. Compute the angle of Nip
   11. Draw the sketch of a single Roll crusher
   12. Describe the working of a single roll crusher
   13. Draw the sketch of a ball mill
   14. Explain the working of ball mill
   15. Compare ball and tube mill
   16. List the factors influencing the size of the product of a ball mill
   17. Derive an equation of critical speed of a ball mill
   18. Compute critical speed
3. Understand the laws of crushing
   1. Explain Rittingers law
   2. State Kicks law
   3. State Bond’s law
   4. Calculate power consumption using Rittingers law
   5. Define particle shape
   6. Define particle size
   7. State mixed particle size
   8. Define specific surface of mixture
   9. Define average particle size
   10. Define shape factorSize Separation
4. Understand size separation
   1. Compare the Tyler and U.S standard screens
   2. List the types of screening equipment
   3. Explain the working of grizzlies
   4. Draw the sketch of a trommel
   5. Explain the working of trommel
   6. Differentiate between shaking and vibrating screen
   7. Draw the sketch of vibrating screen
5. Understand settling methods
   1. List the types of settling
   2. Explain free settling
   3. Derive Stokes law
   4. Calculate terminal settling velocity using Stoke’s law
   5. Explain Hindered settling
   6. Understand the mechanism of fluidization

MODULE III Sedimentation, Agitation & Mixing

1. Understand sedimentation methods
   1. Define sedimentation
   2. Draw the sketches of various stages in Batch sedimentation
   3. Explain Batch sedimentation
   4. Explain continuous sedimentation
   5. Discuss Kynch theory
   6. Explain the determination of thickener area
   7. Draw the sketch of Double cone classifier
   8. State the principle of Jigging
   9. Explain Tabling
2. Understand Floatation methods
   1. Define flotation
   2. Draw the flow sheet of floatation plant using rougher, scavenger and cleaner
   3. Describe flotation equipment
   4. Explain Magnetic separator
3. Understand the working of agitation and mixing equipments
   1. Define Agitation
   2. Distinguish between Agitation and Mixing
   3. List the purpose of agitation
   4. Draw the sketch of an agitation equipment
   5. Explain the working of agitation equipment
   6. Explain the types of Impellors
   7. Draw the sketch of propellers
   8. Explain paddles
   9. Explain the flow pattern in agitated vessels
   10. Explain the function of draft tube and Baffle
   11. Explain the power consumption in agitated vessels
   12. Define power Number.
   13. Define Froude Number.
   14. Calculation of power no, Froude no. and Reynold’s no. with respect to agitation and mixing
   15. Explain dry mixer
   16. Draw the sketch of Banbury mixer
   17. Explain the working of Banbury mixer
   18. Describe ‘V’ type mixer
   19. Describe with a sketch kneading machine

MODULE – IV Fluidisation, Storage and Transportation of Solids, Gases and Liquids

1. Fluidisation
   1. Define fluidization
   2. Discuss the mechanism of fluidization
   3. Describe the characteristics of fluidization
   4. Define minimum fluidization velocity
   5. Define minimum bed height in fluidization
   6. Define the term bed porosity
   7. Discuss the effects of gas velocity on expansion of bed and pressure gradient
   8. List the application of fluidization
   9. Explain with a sketch fluidized bed coal conversion
   10. Describe the fluidized bed oil conversion
   11. Explain phthalic anhydride production
   12. Explain the application of fluidized bed in catalytic cracking with a sketch
   13. Describe application fluidized bed drying
2. Appreciate the storage of solids
   1. Describe hoppers
   2. Explain bins
   3. Explain silos
   4. Define angle of Repose
   5. Discuss the points to be noted in the open storage of solids
3. Understand conveying methods and working of conveyors
   1. Classification of conveyors
   2. Draw the sketches of belt conveyor drives
   3. Explain the belt conveyor construction
   4. Draw the sketch of belt conveyor support belt conveyor idler
   5. Explain belt conveyor take ups
   6. Discuss belt conveyor feeders
   7. Explain belt conveyor discharge methods
   8. Explain chain conveyors
   9. Discuss Apron conveyor
   10. Describe the working of a screw conveyor
   11. Draw the sketch of screw conveyor flight
   12. Compare elevators and chain conveyors
   13. Draw the sketch of a pneumatic
   14. Explain the working of pneumatic conveyor
4. Know the storage of Liquid and gases
   1. Define an atmospheric tank
   2. Sketch some types of roofs of atmospheric storage tank
   3. Define a gasholder
   4. Define pressure vessel in storage of gases
   5. Differentiate between bottles and pipelines in storage of gases

MODULE I Filtration and Centrifugation

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MODULE II Size Reduction

Nature of the materials to be crushed – hardness, structure, moisture content,crushing strength, stickyness, soapyness – explosiveness Types of crusting equipments, coarse crushers -Intermediatecrushers -fine grinders-open circuitgrinding – closed circuit grinding. Laws of crushing – Kick’s law – Rittingers law – Bonds law – Jaw crusher – gyratory – crusher -crushing rolls – angle of nip – simple problems – capacity, hammer mill – ball mill. – critical speed – simple problems – Raymond mill – tube mill. Average particle size – specific surface of mixture, volume surface mean diameter – arithmetic mean diameter – mass mean diameter – shape factor. Size Separation Screens:TylerandU.S.standardscreensScreenanalysis:efficiency and capacity of screens Types of screening equipment – grizzlies – trammels, shaking screens, vibrating screens -separation of solids in liquids. Theory of settling, free and hindered setting – Stoke’s law and its application,terminalvelocities-simpleproblem.

MODULE III Sedimentation, Agitation and Mixing

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MODULE IV

Fluidisation, Storage and Transportation of Solids, Storage of Gases and Liquidization: Mechanism of fluidization – conditions for fluidization – batch fluidization – boiling effect -minimum porosity – bed height – minimum fluidization velocity – effect of gas velocity on expansion of bed and pressure gradient. Characteristics of gas solid fluidized systems – uses of fluidized bed systems – chemical reactors (catalytic and non catalytic) physical contacting drying – classification and conveying Storage and Transportation of Solids, Gases and Liquids Storage of solids – Hoppers – bins – angle of repose. Devices of for discharge of solids -Openstorage of solids Conveyor types – Belt conveyor – Chain conveyor – Scraper conveyor – Apron conveyor -Bucket conveyors – Bucket elevators – Screw conveyors – Pneumatic conveyors – Pneumatic conveying system Auxiliary equipments – Field of application of the above conveyors – Construction and working. Storage of liquid – storage tanks, Storage of volatile liquids – floating roof, Storage of gases: Horton sphere – Wet and Dry specifications and codes for gas storage – Safety precautions.

Reference Books:

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For detailed syllabus of all other subjects of Chemical Engineering, 2015 revision curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

To see the syllabus of all other branches of diploma 2015 revision curriculum do visit all branches of SITTTR diploma 2015 revision.

For Chemical Engineering 6th Sem scheme and its subjects, do visit CH 6th Sem 2015 revision scheme. The detailed syllabus of mass transfer operations ii is as follows.

Course Outcomes:

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SPECIFIC OUTCOMES:

MODULE- I

1. Understand the importance of Leaching.
   1. Define the following terms.
      1. Leaching
      2. Elutriation or Elution
      3. Lixivation.
   2. Differentiate between leaching (solid -liquid extraction) and liquid – Liquid extraction.
   3. Explain the factors affecting rate of solid -liquid extraction.!.1.4 Classify the solid -liquid extraction system.
   4. List the applications of leaching.
   5. Differentiate between batch and continuous leaching operations.
   6. Explain heap leaching.
2. Understand the constructional details and working of extractors.
   1. Explain the working of percolation tank.
   2. Explain the working of Pachuca extractor.
   3. Explain shank system.
   4. Describe the working of agitated vessel with a neat sketch.
   5. Explain the process continuous counter current decantation.
   6. Explain the constructional details and working of Boll man extractor.
   7. Explain the working of a Rotocel extractor with a neat sketch.
   8. Describe the working of a Kennedy extractor with a neat sketch.
   9. Explain the working of Bonotto extractor.
   10. Explain the super critical fluid extraction.

MODULE – II

1. Understand the importance of Liquid -Liquid extraction.
   1. Differentiate between Distillation and Extraction.
   2. Explain the principles of liquid – liquid extraction.
   3. Field of application of Liquid – Liquid extraction.
   4. Explain triangular diagram for Liquid – liquid extraction.
   5. Define distribution Co-efficient and selectivity
   6. Define the terms Raffinate and Extract.
2. Understand the construction details and working of liquid-liquid extractors
   1. Describe the working of spray and packed extraction towers with a sketch.
   2. Explain the working of Mixer settler.
   3. Explain the constructional details and working of Rotating Disk contactor and pulse column .
   4. List the important factors to be considered for selecting a suitable solvent.

MODULE – III

1. Understand the Crystallization in Chemical Industries.
   1. Define Crystallization.
   2. Differentiate between the Evaporation and Crystallization.
   3. Explain the applications of crystallization operation.
   4. Describe the principles of crystallization.
   5. Draw and explain the equilibrium curve for a solid-liquid system.
   6. Define the yield of crystals.
   7. Explain the following terms solubility, saturation, super saturation and rate of crystal growth.
   8. Explain four methods of super saturation.
   9. Derive the material balance equation and solve the simple problems .
   10. Explain the constructional details and working of the tank crystallizer, cooling crystallizer, evaporator crystallizer, Swenson Walker Crystallizer, Krystal crystallizer.
   11. Explain the phenomenon of caking
   12. Define critical humidity and explain the effect of humidity on storage

MODULE- IV

1. Comprehend the principle of rectification.
   1. Draw the layout of distillation column and accessories.
   2. Explain the functions re-boiler and condenser in a distillation column.
   3. List the applications of rectification.
   4. Define an ideal plate.
   5. Prepare material balance and heat balance equation for an ideal plate.
   6. Define constant molal over flow and constant molal vaporizations.
   7. Explain the McCabe & Thiele method.
   8. Derive an equation for rectifying line Derive an equation for stripping line.
   9. Define ‘q’ factor and derive equation for ‘q’ line.
   10. Explain the values of ‘q’ based on five different feed conditions.
   11. Explain the procedure for solving problems using McCabe and Thiele method.
   12. Find the number of theoretical plates required for a given separation and locate the feed plate graphically, and calculate the plate efficiency.
   13. Explain minimum reflux and total reflux.
   14. Estimate graphically the minimum reflux ratio and the minimum number of theoretical plates for rectification.
   15. Differentiate between extractive and azeotropic distillation.
   16. Explain the applications of azeotropic and extractive distillation.
   17. Draw and explain molecular distillation still.
2. Understand the construction of equipments used for various distillation methods.
   1. Describe the construction details of bubble cap columns.
   2. Explain the construction of sieve plate, kittle plate and valve plate.
   3. Define the following terms which affect the efficiency of plate column
      1. Flooding
      2. Entrainment
      3. Weeping
      4. Dumping
      5. Corning

MODULE I

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MODULE II

Definition – Application of Liquid – Liquid extraction – Raffinate – Extract – Triangular diagram -Selectivity – Distribution coefficient- Selection of solvent for extraction- construction details of mixer settlers – Spray tower – packed towers -Sieve tray tower – Rotating disk contactor-Pulse column.

MODULE III

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MODULE IV

Rectification-Definition- principle-application-Fractionating Column-Mechanism fractionation – Concept of ‘q’ – Derivation of q line – Upper operating line – lower operating line – design of a fractionating column by Mccabe-Thiele method – bubble cap column – valve tray – kittle tray- Azeotropic distillationExtractive distillation – molecular distillation.

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For detailed syllabus of all other subjects of Chemical Engineering, 2015 revision curriculum do visit CH 6th Sem subject syllabuses for 2015 revision.

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