JNTUK B.Tech Pharmaceutical Organic Chemistry-I Lab gives you detail information of Pharmaceutical Organic Chemistry-I Lab R13 syllabus It will be help full to understand you complete curriculum of the year.
- Introduction to Equipment & Glassware
- Recrystallization method, determinations of Melting point, Boiling Point and distillation
I. Preparation of organic compounds (each involving a specific organic reaction covered in theory)
- N.Acetylation : Preparation of Acetanilide from Aniline
- 0-Acetylation : Preparation of Aspirin from salicylic acid
- Nuclear Nitration : Preparation of μ-Dinitrobenzene from nitrobenzene
- Oxidation : Preparation of Benzoic acid from Benzyl chloride
- Esterification : Preparation of n-Butyl acetate from n-Butyl alcohol
- Etherification : Preparation of α-Naphthyl methyl ether from α–Naphthol
- Halogenation : Preparation of lodoform from iodation of acetone
- Extensive Nuclear Substitution : Preparation of Tribromophenol
- Bromination of Tribromoaniline from Phenol or Aniline
- II. Systematic qualitative Analysis (Identification) of Monofunctional Organic Compounds
- Avoid water-soluble compounds, and compounds containing more than one functional group; at least six individual compounds to be analyzed.
REFERENCES
- Vogel’s Text Book of Practical Organic Chemistry, 5” Edition.
- R.K. Bansal, Laboratory Manual of Organic Chemistry.
- O.P. Agarwal, Advanced Practical Organic Chemistry.
- F.G.Mann & B.C. Saunders, Practical Organic Chemistry.
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