JNTUK B.Tech Metallurgical Analysis gives you detail information of Metallurgical Analysis R13 syllabus It will be help full to understand you complete curriculum of the year.
Course objective: To study the methods of analysis of various metals and alloys quantitatively and qualitatively.
UNIT-I: (Learning objective: To know the importance of various methods of Metallurgical anaslysis.) Importance of chemical analysis, scope of metallurgical analysis, classification of various methods used in metallurgical analysis. Solution preparations, normality, molarity, molality, Equivalent weight. Dissolution of ores in general, dissolution of metals and alloys.
UNIT-II : (Learning objective: To know the various methods of qualitative analysis of ores and metals) Chemical Analysis – Basic Principles – theory of indicators –Conventional solution methods for qualitative analysis of ores, fluxes, slags, metals and refractories.
UNIT-III: (Learning objective: To know the various methods of qualitative analysis of a few ferrous and non-ferrous metals and alloys ) Qualitative analysis of common non-ferrous alloys such as brasses, bronzes and solders. Estimation of C, S, Si, Mn and P in cast iron and steel.
UNIT-IV: (Learning objective: To estimate various elements present in various ores) Estimation of Cr, Ni, Mo, W and V in alloy steels. Determination of iron in iron ore, manganese in manganese ores, lime in limestone, fire-assay of precious metals.
UNIT-V : (Learning objective: To describe various instrumental methods of analysis and to compare the results with different wet methods) Instrumental analysis: Importance of instrumental analysis –Comparison with standard wet chemical methods – Fundamental Physicochemical principles involved and equipment required in absorptiometry i.e, colorimetry and spectrophotometry, colorimetric titration.
UNIT-VI: (Learning objective: To describe various advanced instrumental methods of analysis) Spectroscopy, potentiometry, amperometric titration. Calorimetric titrations, polarography, conductometry, electro-analysis and flame photometry. (Assessment: The student should be evaluated based on the assignments and objective tests. Emphasis should be given by conducting tutorial classes (with special focus on academically weak students) at the end of each unit).
TEXT BOOK
- S.K.Jain-Metallurgical analysis.
REFERENCES
- Iyer V.G., Metallurgical Analysis: BHU Press, Varanasi.
- Agarwal, B.C. and Jain S.P., A Text Book of Metallurgical Analysis, Khanna Publishers, Delhi -1963.
- Snell Foster D and Frank M Biffen: Commercial methods.of analysis / Che. Publishing Co.,1964
- Vogel Al., A Text Book of Quantitative Inorganic Analysis Longman ELBS 1962.
- Willard H.H.etal: Instrumental Methods of analysis Van Nostrand.
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