JNTUK B.Tech Advanced Separation Technology gives you detail information of Advanced Separation Technology R13 syllabus It will be help full to understand you complete curriculum of the year.
Learning Objectives
- Theoretical and working knowledge of various industrial separation processes
- Theoretical knowledge of advanced distillation with special emphasis towards complex and dividing wall distillation columns.
- Theoretical knowledge of Heat integration of distillation columns
- Theoretical knowledge of Azeotropic distillation; extractive and pressure swing distillation
- Process model development for industrial separation technology
- Elementary knowledge of membrane separation processes
UNIT-I: Characteristics of Separation Processes: Mass and energy agents, Equilibrium processes and rate governed processes, Selection of separation processes factors influencing the choice of a separation process, Degree of freedom analysis for an absorber, two product distillation column, pattern of change in concentration and temperature distribution along the column for binary and multicomponent multistage separations.
Thermodynamic analysis of Processes: Concept of availability and lost work, Calculations on lost work for a simple two product distillation column.
UNIT-II: MESH models for computer solution (only teach hoe the equations are arranged to ease a computer solution, no simulation). Heat integrated and divided wall distillation columns to minimize energy consumption.
UNIT-III: Azeotropic distillation, Extractive distillation and Pressure swing distillation, How to select entrainers for Azeotropic and Extractive distillation, Industrial applications of these distillation techniques.
Residue curve Maps: Introduction, Explaining the concepts using ternary diagrams, Direct and indirect splits, distillation boundaries, Identifying feasible and infeasible products in distillation and their use in selecting entrainers for distillation.
UNIT-IV: Reactive distillation: Introduction, Industrial applications and mathematical model development (Only the model development no simulation)
Batch distillation: Introduction, Industrial applications and mathematical model development using Fenske assumption (Only the model development no simulation).
UNIT-V: Introduction to Multicomponent Absorption; Industrial applications; Model development for Kremser equation solvent loss. Introduction of adsorbers, cryogenic separations, supercritical fluid extraction, chromatographic separations.
UNIT-VI: Introduction to Membrane Separation Technologies; Types of membrane materials; Types of membrane processes: Gas permeation, Reverse osmosis, Microfiltration, Ultrafiltration, Nanofiltration, Electro-dialysis, dialysis; Membrane process models: Solution-diffusion model; Resistances and series model; Concept of concentration polarization; Process design calculations
and industrial applications.
Outcomes
- A student proficient in the Advanced Separation Technology course shall be able to address the
following - For a given separation problem, identify the most relevant separation technology based on physical properties.
- Thermodynamic analysis of distillation columns.
- Working knowledge of complex and dividing wall distillation columns; heat integrated distillation columns; azeotropic, extractive and pressure swing distillation columns.
- For the identified separation technology, carry out process mass balances and design calculations.
- Prominent industrial applications of advanced separation technologies.
- Possible scope for membrane technologies in process industries.
Text Books
- Separation Process, C. Judson King, Mc Graw Hill, 1982.
- Separation Processes Design, J. Sieder and E.J. Henley, Wiley John Sons Publishers, 1998.
- Membrane Separations, M.H.V. Mulder, Springer Publications, 2007.
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