{"id":8313,"date":"2018-08-12T18:50:37","date_gmt":"2018-08-12T18:50:37","guid":{"rendered":"http:\/\/www.inspirenignite.com\/jntuh\/?p=8313"},"modified":"2021-11-05T03:54:31","modified_gmt":"2021-11-05T03:54:31","slug":"jntuh-m-pharm-2017-2018-r17-detailed-syllabus-advanced-instrumental-analysis","status":"publish","type":"post","link":"https:\/\/www.inspirenignite.com\/jntuh\/jntuh-m-pharm-2017-2018-r17-detailed-syllabus-advanced-instrumental-analysis\/","title":{"rendered":"JNTUH M.Pharm 2017-2018 (R17) Detailed Syllabus Advanced Instrumental Analysis"},"content":{"rendered":"<p>Advanced Instrumental Analysis Detailed Syllabus for Pharmaceutical Analysis &amp; Quality Assurance \/ Quality Assurance M.Pharm first year second sem is covered here. This gives the details about credits, number of hours and other details along with reference books for the course.<\/p>\n<p>The detailed syllabus for Advanced Instrumental Analysis M.Pharm 2017-2018 (R17) first year second sem is as follows.<\/p>\n<p>M.Pharm. I Year II Sem.<\/p>\n<p><strong>Course Objectives:<\/strong> This subject deals with various hyphenated analytical instrumental techniques for identification, characterization, and quantification of drugs. Instruments dealtare LC-MS, GC-MS, and hyphenated techniques.<\/p>\n<p><strong>Course Outcome:<\/strong> By the completion of topics the students will come out with the thorough knowledge of various spectral aspects of X-Ray, IR, SEM, ORD etc which help them in further projects works and also industrial opportunities.<\/p>\n<p><strong>UNIT &#8211; I : X-Ray diffraction methods:<\/strong> Origin of X-rays, basic aspects of crystals, X-ray crystallography, miller indices, rotating crystal techniques, single crystal diffraction, power diffraction, structural elucidation and applications.<\/p>\n<p><strong>UNIT &#8211; II<\/strong><\/p>\n<ul>\n<li>Biochromatography: Size exclusion chromatography, ion exchange chromatography, ion pair chromatography, affinity chromatography general principles, stationary phases and mobile phases.<\/li>\n<li>Super critical fluid chromatography: Principles, instrumentation, pharmaceutical applications.<\/li>\n<li>Raman: Principle (absorption, diffraction, scattering and emission of wave, molecular interaction), instrumentation (Dispersive Raman, FT-Raman), advantage and disadvantage, pharmaceutical applications including detection of counterfeit<\/li>\n<\/ul>\n<p><strong>UNIT &#8211; III : Capillary electrophoresis:<\/strong> Overview of CE in pharmaceutical analysis, basic configuration, CE characteristics, principles of CE, methods and modes of CE. General considerations and method Development in CE,<\/p>\n<p><strong>UNIT &#8211; IV<\/strong><\/p>\n<ol>\n<li>DSC: Principle, thermal transitions, instrumentation (Heat flux and power- compensation designs), Modulated DSC, Hyper DSC, experimental parameters (sample preparation, experimental conditions, calibration, heating and cooling rates, resolution, Sources of errors) and their influence, advantages and disadvantages, pharmaceutical applications.<\/li>\n<li>DTA: Principle, instrumentation, advantage and disadvantage, pharmaceutical application, derivative differential thermal analysis (DDTA).<\/li>\n<li>TGA: Principle, instrumentation, factors affecting results, advantages and disadvantages, pharmaceutical application.<\/li>\n<\/ol>\n<p><strong>UNIT &#8211; V<\/strong><\/p>\n<ol>\n<li>Scanning electron microscope (SEM): Principles, Instrumentation and applications.<\/li>\n<li>Optical Rotatory Dispersion (ORD), Circular Dichroism, Cotton effect, Octane rule and applications.<\/li>\n<\/ol>\n<p><strong>REFERENCES:<\/strong><\/p>\n<ol>\n<li>Instrumental Methods of Chemical Analysis by B.K Sharma<\/li>\n<li>Organic spectroscopy by Y.R Sharma<\/li>\n<li>A Text book of Pharmaceutical Analysis by Kerrenth A. Connors<\/li>\n<li>Vogel\u2019s Text book of Quantitative Chemical Analysis by A.I. Vogel<\/li>\n<li>Practical Pharmaceutical Chemistry by A.H. Beckett and J.B. Stenlake<\/li>\n<li>Organic Chemistry by I. L. Finar<\/li>\n<li>Organic spectroscopy by William Kemp<\/li>\n<li>Quantitative Analysis of Drugs by D. C. Garrett<\/li>\n<li>Quantitative Analysis of Drugs in Pharmaceutical Formulations by P. D. Sethi<\/li>\n<li>Spectrophotometric identification of Organic Compounds by Silverstein<\/li>\n<li>HPTLC by P.D. Seth<\/li>\n<li>Spectroscopy by Donald L Pavia, Gary M Lampman, George S Kriz, James A Vyvyan<\/li>\n<\/ol>\n<p><em>For all other M.Pharm 1st Year 2nd Sem syllabus go to\u00a0<a href=\"https:\/\/www.inspirenignite.com\/jntuh\/jntuh-first-year-second-sem-pharmaceutical-analysis-quality-assurance-quality-assurance-course-structure-m-pharmacy-2017-2018-r17-batch\/\">JNTUH\u00a0M.Pharm Pharmaceutical Analysis &amp; Quality Assurance \/ Quality Assurance 1st Year 2nd Sem Course Structure for (R17) Batch.<\/a><\/em><\/p>\n<p>All details and yearly new syllabus will be updated here time to time. Subscribe, like us on facebook and follow us on google plus for all updates.<\/p>\n<p>Do share with friends and in case of questions please feel free drop a comment<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Advanced Instrumental Analysis Detailed Syllabus for Pharmaceutical Analysis &amp; Quality Assurance \/ Quality Assurance M.Pharm first year second sem is covered here. This gives the details about credits, number of [&hellip;]<\/p>\n","protected":false},"author":2259,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_bbp_topic_count":0,"_bbp_reply_count":0,"_bbp_total_topic_count":0,"_bbp_total_reply_count":0,"_bbp_voice_count":0,"_bbp_anonymous_reply_count":0,"_bbp_topic_count_hidden":0,"_bbp_reply_count_hidden":0,"_bbp_forum_subforum_count":0,"footnotes":""},"categories":[154,62],"tags":[],"class_list":["post-8313","post","type-post","status-publish","format-standard","hentry","category-m-pharm","category-syllabus"],"_links":{"self":[{"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/posts\/8313","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/users\/2259"}],"replies":[{"embeddable":true,"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/comments?post=8313"}],"version-history":[{"count":3,"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/posts\/8313\/revisions"}],"predecessor-version":[{"id":13695,"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/posts\/8313\/revisions\/13695"}],"wp:attachment":[{"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/media?parent=8313"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/categories?post=8313"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.inspirenignite.com\/jntuh\/wp-json\/wp\/v2\/tags?post=8313"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}