Pharmaceutical Organic Chemistry-I Lab Detailed Syllabus for B.Tech first year first sem is covered here. This gives the details about credits, number of hours and other details along with reference books for the course.
The detailed syllabus for Pharmaceutical Organic Chemistry-I Lab B.Tech 2016-2017 first year fristsem is as follows.
B.Pharm. I Year I Sem. L T/P/D C
Course Code: BS109 0 0/3/0 2
I. Introduction to Equipment and Glassware
- Determination of melting point/boiling point by Thiels method.
- Determination of Mixed melting point for organic compounds.
- Recrystallization (Purification including decolourization) of two organic compounds.
- Purification and drying of organic solvents.
II. Preparation of organic compounds (each involving a specific organic reaction covered in theory)
- N-Acetylation : Preparation of Acetanilide from Aniline
- O-Acetylation : Preparation of Aspirin from Salicylic acid
- Nuclear Bromination : Preparation of p-Bromoacetanilide from Acetanilide
- Hydrolysis : Preparation of p-Bromoaniline from p-Bromoacetanilide
- Nuclear Nitration : Preparation of m-Dinitrobenzene from nitrobenzene
- Oxidation : Preparation of Benzoic acid from Benzyl chloride
- Esterification : Preparation of n-Butylacetate from n-Butylalcohol
- Etherification : Preparation of (a) Naphthyl methyl ether from (b) Naphthol (c) Halogenation : Preparation of Iodoform from Oxidation of Acetone
- Extensive Nuclear : Preparation of Tribromophenol or Bromination Substitution Tribromoaniline from Phenol or Aniline
Systematic qualitative Analysis (Identification) of Monofunctional Organic Compounds: Avoid water-soluble compounds, and compounds containing more than one functional group; at least six individual compounds to be analyzed.
References
- Vogel’s Text Book of Practical Organic Chemistry, 5th Edition.
- R. K. Bansal, Laboratory Manual of Organic Chemistry.
- P. Agarwal Advanced Practical Organic Chemistry.
- F. G. Mann and B.C. Saunders, Practical Organic Chemistry.
- Organic Chemistry a lab manual, Cengage learning India Pvt. Ltd. By Pavia
- Advanced Practical Organic Chemistry, Vishoi-Vikas Publications.
All details and yearly new syllabus will be updated here time to time. Subscribe, like us on facebook and follow us on google plus for all updates.
Do share with friends and in case of questions please feel free drop a comment.